Pretreatment Effect on the Properties of the Cr-Mg Catalyst for the Gas-Phase Hydrofluorination of Perchloroethylene into Pentafluoroethane

Petrov R. V.; Zirka A. A.; Reshetnikov S. I.

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Pretreatment Effect on the Properties of the Cr-Mg Catalyst for the Gas-Phase Hydrofluorination of Perchloroethylene into Pentafluoroethane

机译：对氯乙烯加入五氟乙烷的气相氢化的Cr-Mg催化剂的预处理作用

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The effect of the temperature of thermal pretreatment of the precursors of the Cr-Mg catalyst on its physicochemical properties (specific surface area and elemental composition) and catalytic properties has been experimentally investigated. The dehydration of the precursor takes place up to a temperature of similar to 500 degrees C, making it possible to tune the catalyst composition by varying the heat-treatment temperature. The samples prepared from precursors with various compositions differ in their specific surface area and catalytic activity. The highest activity is shown by the catalyst prepared by heat treatment of the precursor at 330 degrees C.

机译：通过实验研究了CR-Mg催化剂前体的热预处理的温度对其物理化学性质（比表面积和元素组成）和催化性质的影响。前体的脱水发生高达500℃的温度，使得可以通过改变热处理温度来调谐催化剂组合物。用各种组合物制备的样品在其特异性表面积和催化活性方面不同。通过在330℃下通过前体的热处理制备的催化剂显示最高活性。

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《Kinetics and catalysis》 |2017年第4期|共5页
作者
Petrov R. V.; Zirka A. A.; Reshetnikov S. I.;
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作者单位

Russian Acad Sci Siberian Branch Boreskov Inst Catalysis Novosibirsk 630090 Russia;

Russian Acad Sci Siberian Branch Boreskov Inst Catalysis Novosibirsk 630090 Russia;

Russian Acad Sci Siberian Branch Boreskov Inst Catalysis Novosibirsk 630090 Russia;

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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
gas-phase hydrofluorination; pentafluoroethylene; chromium-magnesium catalyst;

机译：气相氢氟化;五氟乙烯;铬 - 镁催化剂;

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1. Pretreatment Effect on the Properties of the Cr-Mg Catalyst for the Gas-Phase Hydrofluorination of Perchloroethylene into Pentafluoroethane [J] . Petrov R. V., Zirka A. A., Reshetnikov S. I. Kinetics and catalysis . 2017,第4期

机译：对氯乙烯加入五氟乙烷的气相氢化的Cr-Mg催化剂的预处理作用
2. Determination of Parameters of a Mathematical Model for Regeneration of a Chromium-Aluminum Catalyst for Gas-Phase Perchloroethylene Hydrofluorination into Pentafluoroethane (Freon 125) [J] . R. V. Petrov, A. A. Zirka, S. I. Reshetnikov Kinetics and catalysis . 2013,第5期

机译：气相全氯乙烯氢氟化成五氟乙烷的铬铝催化剂的再生数学模型的参数确定（氟利昂125）
3. Kinetics study of the perchloroethylene hydrofluorination into pentafluoroethane (Freon 125) over chromium-based catalyst [J] . A.A. Zirka, R.V. Petrov, S.I. Reshetnikov Chemical engineering journal . 2011,第Null期

机译：铬基催化剂上全氯乙烯氢氟化为五氟乙烷（Freon 125）的动力学研究
4. Effect Of Chromium Content On The Properties Of A Alumina-Chromia Catalyst In Tetrachloroethylene Hydrofluorination [C] . Roman Petrov, Alexander Zirka, Sergey Reshetnikov International Conference of Students and Young Scientists"Prospects of Fundamental Sciences Development" . 2016

机译：铬含量对四氯乙烯氢氟化氧化铝 - 铬催化剂性能的影响
5. THE EFFECTS OF PRETREATMENT ON THE BEHAVIOR OF PLATINUM/RHENIUM/ALUMINA CATALYSTS [D] . ISAACS, BRUCE HARTMAN 1981

机译：预处理对铂/ R /铝催化剂行为的影响
6. Catalytic Dechlorination of Gas-phase Perchloroethylene under Mixed Redox Conditions [O] . Özer Orbay, Song Gao, Brian Barbaris, -1

机译：混合氧化还原条件下气相全氯乙烯的催化脱氯
7. Determination of the factors that affect the gas-phase reactivity of metal-centered cyclopropanation catalysts and examination of the properties of their reaction products [O] . Aldajaei Jamal 2014

机译：确定影响金属中心环丙烷化催化剂气相反应性的因素并检查其反应产物的性质
8. Metabolism of Perchloroethylene and 1,1,1,2-Tetrachloroethane After Carbon Tetrachloride Pretreatment in B6C3F1 Mice [R] . Mahle, D. A. , Godfrey, R. J. , Buttler, G. W. , 2000

机译：B6C3F1小鼠四氯化碳预处理后全氯乙烯和1,1,1,2-四氯乙烷的代谢

Pretreatment Effect on the Properties of the Cr-Mg Catalyst for the Gas-Phase Hydrofluorination of Perchloroethylene into Pentafluoroethane

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