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首页> 外文期刊>Physics of the solid state >Formation of the atomically ordered L1(0) structure with the [001] orientation during the solid-state reaction in Fe/Pd bilayer thin films
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Formation of the atomically ordered L1(0) structure with the [001] orientation during the solid-state reaction in Fe/Pd bilayer thin films

机译:在Fe / Pd双层薄膜中的固态反应期间,形成原子序的L1(0)结构与[001]取向

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摘要

The formation of the atomically ordered L1(0)-FePd structure during the solid-state reaction in Fe/Pd bilayer thin films is in situ investigated by electron microscopy and electron diffraction analysis. The initial iron and palladium layers were mainly coherently oriented crystallites with the orientation relationship alpha-Fe (001)[110] || Pd(001)[100]. It is established that the solid-state reaction between the iron and palladium layers upon heating at a rate of 4-8A degrees C/min starts with the formation of the FePd solid solution at 390A degrees C; at 430A degrees C, the formation of the atomically ordered L1(0)-FePd structure is observed. It is shown that at the low heating rate (4-8A degrees C/min), the L1(0)-FePd structure with the [001] orientation relative to the film plane forms, while at the high heating rate (50A degrees C/min) it forms with the [100], [010], and [001] orientations.
机译:通过电子显微镜和电子衍射分析,在Fe / Pd双层薄膜中的固态反应期间形成原子排序的L1(0)-Fepd结构。 初始钢和钯层主要是连贯定向的微晶,具有方向关系α-Fe(001)[110] || PD(001)[100]。 建立铁和钯层在加热时的固态反应以4-8A的速度加热,以390A℃的FEPD固溶体的形成开始; 在430A℃下,观察到原子序的L1(0)-Fepd结构的形成。 结果表明,在低加热速率(4-8A℃/ min),L1(0) - 具有相对于膜平面形式的[001]取向的L1(0)的结构,同时以高加热速度(50A度C. / min)用[100],[010]和[001]形式形成。

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