One-Pot, Sequential Four-Component Synthesis of Benzo[a]chromeno[2,3-c]phenazine Derivatives Using SiO2-SO3H as an Efficient and Recoverable Catalyst Under Conventional Heating and Microwave Irradiation

Yazdani-Elah-Abadi Afshin; Mohebat Razieh; Maghsoodlou Malek-Taher; Heydari Reza

首页> 外文期刊>Polycyclic Aromatic Compounds: The Journal of International Society for Polycyclic Aromatic Compounds >One-Pot, Sequential Four-Component Synthesis of Benzo[a]chromeno[2,3-c]phenazine Derivatives Using SiO2-SO3H as an Efficient and Recoverable Catalyst Under Conventional Heating and Microwave Irradiation

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One-Pot, Sequential Four-Component Synthesis of Benzo[a]chromeno[2,3-c]phenazine Derivatives Using SiO2-SO3H as an Efficient and Recoverable Catalyst Under Conventional Heating and Microwave Irradiation

机译：使用SiO2-SO3H在常规加热和微波辐射下，使用SiO2-SO3H作为一种有效且可回收的催化剂，苯并[A] Chromeno [2,3-C]吩嗪衍生物的单壶。

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Silica sulfuric acid (SiO2-SO3H) has been used as an effective and reusable solid catalyst for the one-pot, two-step, four-component microwave-assisted synthesis of benzo[a]chromeno[2,3-c]phenazine derivatives by the condensation reaction of 2-hydroxynaphthalene-1,4-dione, o-phenylenediamine, aldehydes, and cyclic 1,3-dicarbonyl compounds. This new procedure has a number of advantages such as: high yields, very short reaction time, operational simplicity, simple work-up procedures and avoidance of hazardous or toxic catalysts, and organic solvents and is devoid of inessential derivatization and generation of hazardous substances. Moreover, the catalyst shows high thermal stability and can be recovered and reused without loss of reactivity.

机译：二氧化硅硫酸（SiO 2-SO3H）已被用作一锅，两步，四组分微波辅助合成苯并[A] Chromeno [2,3-C]苯脲衍生物的有效和可重复使用的固体催化剂通过2-羟基萘-1,4-二酮，O-苯二胺，醛和环状1,3-二羰基化合物的缩合反应。这种新程序具有许多优点，如：高产率，反应时间短，操作简单，操作简单，简单的后处理程序和避免危险或有毒催化剂，以及有机溶剂，并且具有非态度衍生化和产生有害物质的产生。此外，催化剂显示出高热稳定性，并且可以在不损失反应性的情况下回收并重复使用。

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来源
《Polycyclic Aromatic Compounds: The Journal of International Society for Polycyclic Aromatic Compounds》 |2018年第1期|共10页
作者
Yazdani-Elah-Abadi Afshin; Mohebat Razieh; Maghsoodlou Malek-Taher; Heydari Reza;
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作者单位

Univ Sistan &

Baluchestan Dept Chem Fac Sci POB 98135 674 Zahedan Iran;

Islamic Azad Univ Yazd Branch Dept Chem Yazd Iran;

Univ Sistan &

Baluchestan Dept Chem Fac Sci POB 98135 674 Zahedan Iran;

Univ Sistan &

Baluchestan Dept Chem Fac Sci POB 98135 674 Zahedan Iran;

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原文格式 PDF
正文语种 eng
中图分类石油、天然气加工工业;化学工业;
关键词
Benzoachromeno2; 3-cphenazine; microwave irradiation; multi-component reactions (MCRs); silica sulfuric acid (SSA);

机译：苯并[A] Chromeno [2;3-C]苯氮杂物;微波辐照;多组分反应（MCR）;二氧化硅硫酸（SSA）;

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1. One-Pot, Sequential Four-Component Synthesis of Benzo[a]chromeno[2,3-c]phenazine Derivatives Using SiO2-SO3H as an Efficient and Recoverable Catalyst Under Conventional Heating and Microwave Irradiation [J] . Yazdani-Elah-Abadi Afshin, Mohebat Razieh, Maghsoodlou Malek-Taher, Polycyclic Aromatic Compounds: The Journal of International Society for Polycyclic Aromatic Compounds . 2018,第1期

机译：使用SiO2-SO3H在常规加热和微波辐射下，使用SiO2-SO3H作为一种有效且可回收的催化剂，苯并[A] Chromeno [2,3-C]吩嗪衍生物的单壶。
2. One-pot, sequential four-component synthesis of benzo[c]pyrano[3,2-a]phenazine, bis-benzo[c]pyrano[3,2-a]phenazine and oxospiro benzo[c]pyrano[3,2-a]phenazine derivatives using 1,4-diazabicyclo[2.2.2]octane (DABCO) as an efficient and reusable solid base catalyst [J] . Alireza Hasaninejad, Somayeh Firoozi Molecular Diversity . 2013,第3期

机译：一锅顺序四组分合成苯并[c]吡喃并[3,2-a]吩嗪，双苯并[c]吡喃并[3,2-a]吩嗪和氧螺环苯并[c]吡喃[3,2] -a]吩嗪衍生物，使用1,4-二氮杂双环[2.2.2]辛烷（DABCO）作为有效且可重复使用的固体基础催化剂
3. A Rapid and Highly Efficient Microwave-Promoted Four-Component Domino Reaction for the Synthesis of Novel Spiro[benzo[a]chromeno[2,3-c]phenazine] Derivatives Under Solvent-Free Conditions [J] . Mohebat Razieh, Simin Nasim, Yazdani-Elah-Abadi Afshin Polycyclic Aromatic Compounds: The Journal of International Society for Polycyclic Aromatic Compounds . 2019,第2期

机译：一种快速且高效的微波促进的四组分Domino反应，用于合成新的螺螺（苯并[A] Chromeno [2,3-C]吩嗪）衍生物在无溶剂条件下
4. Efficient One-Pot Synthesis of 12-Aryl-8,9,10,12-tetrahydrobenzoaxanthen-11-one Derivatives Using NaHSO4 as Catalyst in Ionic Liquid [C] . Hong Jun Zang, Yong Zhang, Bo-Wen Cheng EMEM 2010;International conference of environment materials and environment management . 2010

机译：NaHSO4在离子液体中的催化剂高效单锅合成12-芳基-8,9,10,12-四氢苯并a黄嘌呤-11-one衍生物
5. ZnO Nanoparticles as an Efficient Heterogeneous Reusable and Ecofriendly Catalyst for Four-Component One-Pot Green Synthesis of Pyranopyrazole Derivatives in Water [O] . Harshita Sachdeva, Rekha Saroj 2013

机译：ZnO纳米颗粒作为高效多相可重复使用和生态友好的催化剂用于水中的吡喃并吡唑衍生物的四组分一锅法绿色合成
6. Synthesis of one-pot pyrazolo4′,3′:5,6pyrano2,3-cphenazin-15-yl) methanone derivatives via a multi-component using Fe3O4@TiO2-SO3H as a recoverable magnetic catalyst under microwave irradiation [O] . Milad Taheri, Razieh Mohebat 2020

机译：使用Fe 3 O 4 -TiO2-So3H作为可回收磁性催化剂，通过多组分合成单壶吡唑4'，3'，3'：5,6甲酮衍生物的甲基酮衍生物微波辐照

One-Pot, Sequential Four-Component Synthesis of Benzo[a]chromeno[2,3-c]phenazine Derivatives Using SiO2-SO3H as an Efficient and Recoverable Catalyst Under Conventional Heating and Microwave Irradiation

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