Nano-NiZr4(PO4)6 as a superior catalyst for the synthesis of propargylamines under ultrasound irradiation

HosseinShahbazi-Alavi; Seyed HadiNazemzadeh; AbolfazlZiarati; JavadSafaei-Ghomi

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Nano-NiZr4(PO4)6 as a superior catalyst for the synthesis of propargylamines under ultrasound irradiation

机译：纳米NizR4（PO4）6作为在超声辐射下合成丙氨酸的优异催化剂

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An easy and rapid method for the synthesis of propargylamines has been achieved through a three-component reaction of phenylacetylene, aromatic aldehydes, and morpholine or piperidine using nano-NiZr4(PO4)6 under ultrasound irradiation. Atom economy, a wide range of products, excellent yields in short times, reusability of the catalyst, and low catalyst loading are some of the important features of this protocol.

机译：通过在超声辐射下，通过使用纳米-NizR4（PO4）6在超声辐射下通过苯乙炔，芳香族醛和吗啉或哌啶或哌啶的三分组分反应来实现一种简单且快速的丙酰胺的方法。原子经济，广泛的产品，在短时间内产量优异，催化剂的可重用性，低催化剂负载是本方案的一些重要特征。

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来源
《Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences》 |2018年第4期|共5页
作者
HosseinShahbazi-Alavi; Seyed HadiNazemzadeh; AbolfazlZiarati; JavadSafaei-Ghomi;
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作者单位

Department of Organic Chemistry Faculty of Chemistry University of Kashan P. O. Box 87317-51167 Kashan I. R. Iran Tel.: +98 31 55427233 Fax: +98 31 55427233;

Department of Organic Chemistry Faculty of Chemistry University of Kashan P. O. Box 87317-51167 Kashan I. R. Iran;

School of Chemistry College of Science University of Tehran Tehran 14155-6455 I. R. Iran;

Department of Organic Chemistry Faculty of Chemistry University of Kashan P. O. Box 87317-51167 Kashan I. R. Iran;

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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
nanocatalyst; one-pot synthesis; phenylacetylene; propargylamine; ultrasonic conditions;

机译：纳米催化剂;单罐合成;苯乙烯;丙基丙胺;超声波条件;

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专利

1. Nano-NiZr4(PO4)6 as a superior catalyst for the synthesis of propargylamines under ultrasound irradiation [J] . HosseinShahbazi-Alavi, Seyed HadiNazemzadeh, AbolfazlZiarati, Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences . 2018,第3a4期

机译：纳米NizR4（PO4）6作为在超声辐射下合成丙氨酸的优异催化剂
2. Synthesis of pyrimidines using nano-NiZr4 (PO4)6 as a retrievable and robust heterogeneous catalyst [J] . Shahbazi-Alavi Hossein, Safaei-Ghomi Javad Nanochemistry Research . 2020,第2期

机译：使用纳米氮（PO4）6合成嘧啶，作为可检索且鲁棒的非均相催化剂
3. Synthesis of new 2-amino-4H-pyran-3,5-dicarboxylate derivatives using nanocrystalline (MZr4)-Zr-II(PO4)(6) ceramics as reusable and robust catalysts under microwave irradiation [J] . Safaei-Ghomi Javad, Javidan Abdollah, Ziarati Abolfazl, Journal of nanoparticle research: An interdisciplinary forum for nanoscale science and technology . 2015,第8期

机译：使用纳米晶体（MZr4）-Zr-II（PO4）（6）陶瓷作为微波辐射下可重复使用且坚固的催化剂，合成新的2-氨基-4H-吡喃-3,5-二羧酸酯衍生物
4. Effects of Ultrasound Irradiation on Synthesis of Solid Acid Catalysts [C] . Mariam Arneen, Mohd Tazli Azizan, Suzana Yusup International Conference on Science and Engineering of Materials . 2016

机译：超声辐照对固体酸催化剂合成的影响
5. Application of microwave irradiation and solid acid catalysts in environmental organic chemistry. Synthesis and reactivity of heterocycles. [D] . Vazquez Fernandez-Pacheco, Ester. 2000

机译：微波辐射和固体酸催化剂在环境有机化学中的应用。杂环的合成和反应性。
6. In Situ Immobilized Silver Nanoparticles on Rubiatinctorum Extract-Coated Ultrasmall Iron OxideNanoparticles: An Efficient Nanocatalyst with Magnetic Recyclabilityfor Synthesis of Propargylamines by A3 Coupling Reaction [O] . Hojat Veisi, *, Lida Mohammadi, 2019

机译：原位固定化的银纳米粒子在茜草属上锡提取物涂层超细氧化铁纳米颗粒：具有磁可回收性的高效纳米催化剂A3偶联反应合成炔丙胺
7. Nano magnetite (Fe3O4), an efficient and robust catalyst for the one-pot synthesis of 1-(aryl(piperidin-1-yl)methyl)naphthalene-2-ol and 1-(α-amido alkyl)-2-naphthol under ultrasound irradiation [O] . Masoud Mokhtary, Mogharab Torabi 2017

机译：纳米磁铁矿（Fe3O4），一锅法合成1-（芳基（哌啶-1-基）甲基）萘-2-醇和1-（α-酰氨基烷基）-2-萘酚的高效稳健催化剂超声辐射

Nano-NiZr4(PO4)6 as a superior catalyst for the synthesis of propargylamines under ultrasound irradiation

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