Synthesis and characterization of K5Sn2OF11

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Synthesis and characterization of K5Sn2OF11

机译：K5SN2OF11的合成与表征

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The potassium oxidofluoridostannate(IV) fluoride K5Sn2OF11 was synthesized via a solid-state route at T?=?300°C in arc-weldeded copper ampoules. It crystallizes in the orthorhombic system in the acentric space group Ama2 (no. 40) with a unit cell volume of V?=?2.5727(4) nm3. The cell parameters are a?=?1758.3(2), b?=?2452.3(2) and c?=?596.7(1) pm. As a main structural motif, K5Sn2OF11 exhibits two different kinds of dinuclear [Sn2OF11]5? units, which are embedded into a matrix consisting of potassium cations and fluoride anions. The substance was characterized by single-crystal and powder X-ray diffraction, as well as by FT-IR spectroscopy.

机译：通过在弧焊铜安瓿中的固态途径合成氧化氧化氢硼酸盐（IV）氟化物K5SN2OF11。它在龈核空间组AMA2（NO.40）中的正交系统中结晶，单位细胞体积为v？= 2.5727（4）NM3。细胞参数是a？=？1758.3（2），B？= 2452.3（2）和C？=？596.7（1）PM。作为主要的结构图案，K5SN2OF11展示了两种不同类型的Dinuclear [Sn2OF11] 5？单位嵌入到由钾阳离子和氟阴离子组成的基质中。该物质的特征在于单晶和粉末X射线衍射，以及FT-IR光谱。

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《Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences》 |2020年第2期|共8页
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正文语种 eng
中图分类化学;
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crystal structure; FT-IR spectroscopy; potassium oxidofluoridostannate(IV) fluoride;

机译：晶体结构;FT-IR光谱;氧化氧化氢氧化钾（IV）氟化物;

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Synthesis and characterization of K5Sn2OF11

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