Bis(triphenylphosphoranylidene)ammonium tetraethylborate, (Ph3P)(2)N+BEt4-: preparation and structure

Cameron TS.; Peach ME.

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Bis(triphenylphosphoranylidene)ammonium tetraethylborate, (Ph3P)(2)N+BEt4-: preparation and structure

机译：双（三苯基膦基）四乙基硼酸铵，（pH3p）（2）n + Bet4-：制备和结构

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The compound (Ph3P)(2)N+BEt4- is readily prepared from (Ph3P)(2)N+Cl- and LiBHEt3. The NMR spectrum (H-1, C-13, B-11, P-33) are reported. C44H50NBP2, M = 665.64, Triclinic, P (1) over bar (#2), a = 11.530(4), b = 15.397(9), c = 11.497(9) Angstrom, alpha = 102.94(6), beta = 102.87(4), gamma = 89.34(4)degrees, V = 1938(4) Angstrom(3), and Z = 2. [References: 16]

机译：化合物（PH3P）（2）N + Bet4-易于由（PH3P）（2）N + Cl-和LibHet3制备。报道了NMR光谱（H-1，C-13，B-11，P-33）。 C44H50NBP2，M = 665.64，三级，P（1）上棒（＃2），a = 11.530（4），B = 15.397（9），C = 11.497（9）埃，α= 102.94（6），β= 102.87（4），γ= 89.34（4）度，v = 1938（4）埃（3）和Z = 2. [参考：16]

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《Journal of chemical crystallography》 |1998年第12期|共6页
作者
Cameron TS.; Peach ME.;
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作者单位

Dalhousie Univ Dept Chem Halifax NS B3H 4J3 Canada.;

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原文格式 PDF
正文语种 eng
中图分类晶体学;
关键词
Bet4- anion; Complex cations; Crystal; Complex;

机译：Bet4-阴离子;复杂阳离子;水晶;复杂;

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1. Bis(triphenylphosphoranylidene)ammonium tetraethylborate, (Ph3P)(2)N+BEt4-: preparation and structure [J] . Cameron TS., Peach ME. Journal of chemical crystallography . 1998,第12期

机译：双（三苯基膦基）四乙基硼酸铵，（pH3p）（2）n + Bet4-：制备和结构
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机译：聚磺胺。 CLXXVIII。苯1,2,2-二（磺酰基）胺（HZ）的鎓盐：铵盐NH（4）Z（。）H（2）O的第二种晶体形式和双（三苯基磷杂亚基）铵盐的晶体结构[Ph3PNPPh3] Z
3. The Preparation and Crystal Structure of Ammonium Bismuth (III) Thiosalicylate Dihydrate [J] . Dalius S. Sagatys, Grahan Smith, Raymond C. Bott, Australian Journal of Chemistry: A Journal for the Publication of Original Research in All Branches of Chemistry . 2003,第9期

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5. THE HYDROTHERMAL PREPARATION AND X-RAY CRYSTAL STRUCTURE DETERMINATION OFSOME COPPER(I) AND COPPER(II) AMMONIUM HALIDES. [D] . CLAYTON, WILLIAM REX. 1971

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6. Bis(benzyltrimethylammonium) bis(4SR12SR18RS26RS)-41826-trihydroxy-12-oxido-1317-dioxaheptacyclo14.10.0.0314.0412.0611.01826.01924hexacosa-13(14)681015192123-nonaene-525-dione sesquihydrate: dimeric structure formation via O—H—O−negative charge-assisted hydrogen bonds (–CAHB) with benzyltrimethylammonium counter-ions [O] . Ravell Bengiat, Maayan Gil, Asne Klein, 2016

机译：双（苄基三甲基铵）双（4SR12SR18RS26RS）-41826-三羟基-12-氧化物-1317-二氧杂庚环14.10.0.0314.0412.0611.01826.01924 hexacosa- 13（14）681015192123-壬二烯-525-二酮倍半水合物：通过OH-O-形成二聚体结构负电荷辅助氢键（–CAHB）与苄基三甲基铵抗衡离子
7. Coordination Chemistry of Perhalogenated Cyclopentadienes and Alkynes. 17. Reaction of Dichloroethyne With Platinum(0) Phosphine Complexes: Formation of a .pi.-Complex, Isomerization to .beta.-Chloroethynyl Complexes, and Syntheses of Diplatinioethyne Derivatives. Molecular Structures of (Ph3P)2Pt(.eta.2-ClC.tplbond.CCl) and Cl(Ph3P)2PtC.tplbond.CPt(PPh3)2Cl [O] . Sünkel Karlheinz, Birk Uwe, Robl Christian 1994

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Bis(triphenylphosphoranylidene)ammonium tetraethylborate, (Ph3P)(2)N+BEt4-: preparation and structure

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