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首页> 外文期刊>Journal of mass spectrometry: JMS >Entrapment of amino acids in gas phase surfactant assemblies: The case of tryptophan confined in positively charged (1 RR ,2 SS )‐dodecyl (2‐hydroxy‐1‐methyl‐2‐phenylethyl) dimethylammonium bromide aggregates
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Entrapment of amino acids in gas phase surfactant assemblies: The case of tryptophan confined in positively charged (1 RR ,2 SS )‐dodecyl (2‐hydroxy‐1‐methyl‐2‐phenylethyl) dimethylammonium bromide aggregates

机译：诱捕气相表面活性剂组件中的氨基酸：色氨酸的情况局限性（1 R r，2 s s） - 二癸基（2-羟基-1-甲基-2-苯基乙基）二甲基溴化物聚集体

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Abstract > The ability of positively charged aggregates of the surfactant (1 <fi>R</fi> ,2 <fi>S</fi> )‐dodecyl(2‐hydroxy‐1‐methyl‐2‐phenylethyl)dimethylammonium bromide (DMEB) to incorporate D‐tryptophan or L‐tryptophan in the gas phase has been investigated by electrospray ion mobility mass spectrometry (ESI‐IM‐MS). Strongly impacted by the pH of the electrosprayed solutions, both protonated (T + ) and deprotonated (T ? ) tryptophan are effectively included into the aggregates, whereas, tryptophan in zwitterionic (T 0 ) form is practically absent in singly charged DMEB aggregates but can be found in multiply charged ones. The ability to incorporate tryptophan increases with the aggregation number and charge state of aggregates. More than 1 tryptophan species can be entrapped (aggregates including up to 5 tryptophan are observed). > Collision induced dissociation experiments performed on the positively singly charged DMEB hexamer containing 1 T ? show that at low collision energies the loss of a DMEB molecule is preferred with respect to the loss of the DMEB cation plus T ? species which, in turn, is preferred with respect to the loss of mere tryptophan, suggesting that the deprotonated amino acid is preferentially located in proximity of a DMEB head group and with the ionic moiety pointing towards the core of the aggregate. >The analysis of the collision cross sections (CCS) of bare and tryptophan containing aggregates allowed evaluating the contributions of tryptophan and bromide ions to the total aggregate CCS. No significant discrimination between D‐tryptophan and L‐tryptophan by the chiral DMEB aggregates has been evidenced by mass spectra data, CID experiments, and CCS values. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract xmlns =“http://www.wiley.com/namespaces/wiley”type =“main”> <title type =“main”>抽象</ title> >表面活性剂的带正电荷聚集的能力（1 <fi> R </ fi>，2 <fi> s </ fi>） - 二癸基（2-羟基-1-甲基-2-苯乙基）二甲基溴（DMEB）掺入D-色氨酸或L-色氨酸通过电喷雾离子迁移率质谱（ESI-IM-MS）研究了气相。由电喷雾溶液的pH强烈影响，质子化（T <SUP> + </ sup>）和质子化（T β-sup>）色氨酸有效地纳入聚集体中，而在两性离子的色氨酸（ T <SUP> 0 </ sup>）形式实际上在单电压的DMEB聚集体中缺席，但可以在乘法收费中找到。结合色氨酸的能力随着聚集体的聚合数和电荷状态而增加。可以捕获超过1种色氨酸物种（观察到包括多达5色氨酸的聚集体）。碰撞诱导在含有1T 的正单电荷的DMEB六聚体上进行的解离实验表明，在低碰撞能量下，对于损失，优选DMEB分子的丧失DMEB阳离子加T <SUP>α</ sup>又是关于仅仅是单纯色氨酸的损失优选的物种，表明所述去质子化氨基酸优先位于DMEB头部和离子的邻近指向骨料核心的部分。 </ p> >裸露和色氨酸含有聚集体的碰撞横截面（CCS）的分析允许评估色氨酸和溴离子的贡献给总骨料CCS。 Chiral DMEB聚集体的D-色氨酸和L-色氨酸之间没有显着的歧视已经通过质谱数据，CID实验和CCS值证明了。</ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-34906/'>《Journal of mass spectrometry: JMS》</a> <b style="margin: 0 2px;">|</b><span>2017年第10期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bongiorno David&option=202" target="_blank" rel="nofollow">Bongiorno David;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Calabrese Valentina&option=202" target="_blank" rel="nofollow">Calabrese Valentina;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ceraulo Leopoldo&option=202" target="_blank" rel="nofollow">Ceraulo Leopoldo;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Indelicato Serena&option=202" target="_blank" rel="nofollow">Indelicato Serena;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Turco Liveri Vincenzo&option=202" target="_blank" rel="nofollow">Turco Liveri Vincenzo;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Dipartimento di Scienze e Tecnologie Biologiche Chimiche e Farmaceutiche (STEBICEF)Università degli Studi di PalermoVia Archirafi 32 90123 Palermo Italy;</p> <p>Dipartimento di Scienze e Tecnologie Biologiche Chimiche e Farmaceutiche (STEBICEF)Università degli Studi di PalermoVia Archirafi 32 90123 Palermo Italy;</p> <p>Dipartimento di Scienze e Tecnologie Biologiche Chimiche e Farmaceutiche (STEBICEF)Università degli Studi di PalermoVia Archirafi 32 90123 Palermo Italy;</p> <p>Dipartimento di Scienze della Terra e del Mare (DISTEM)Università degli Studi di Palermovia Archirafi 26 90123 Palermo Italy;</p> <p>Dipartimento di Scienze e Tecnologie Biologiche Chimiche e Farmaceutiche (STEBICEF)Università degli Studi di PalermoVia Archirafi 32 90123 Palermo Italy;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1187.html" title="分析化学">分析化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=DMEB&option=203" rel="nofollow">DMEB;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=gas‐phase self‐assembly&option=203" rel="nofollow">gas‐phase self‐assembly;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ion mobility&option=203" rel="nofollow">ion mobility;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=surfactant aggregates&option=203" rel="nofollow">surfactant aggregates;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=tryptophan&option=203" rel="nofollow">tryptophan;</a> </p> <div class="translation"> 机译：DMEB;气相自组装;离子迁移率;表面活性剂聚集体;色氨酸; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025633242.html">Entrapment of amino acids in gas phase surfactant assemblies: The case of tryptophan confined in positively charged (1 <i xmlns="http://www.wiley.com/namespaces/wiley">RR ,2 <i xmlns="http://www.wiley.com/namespaces/wiley">SS )‐dodecyl (2‐hydroxy‐1‐methyl‐2‐phenylethyl) dimethylammonium bromide aggregates</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bongiorno David&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Bongiorno David,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Calabrese Valentina&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Calabrese Valentina,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ceraulo Leopoldo&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Ceraulo Leopoldo,</a> <a href="/journal-foreign-34906/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of mass spectrometry: JMS .</a> <span>2017</span><span>,第10期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：诱捕气相表面活性剂组件中的氨基酸：色氨酸的情况局限性（1 <i xmlns =“http://www.wiley.com/namespaces/wiley”> R </ i> r，2 <i XMLNS =“http://www.wiley.com/namespaces/wiley”> s </ i> s） - 二癸基（2-羟基-1-甲基-2-苯基乙基）二甲基溴化物聚集体</span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704024020378.html">Gas‐phase chemical ionization of 4‐alkyl branched‐chain carboxylic acids and 3‐methylindole using H <sub xmlns="http://www.wiley.com/namespaces/wiley">3</sub>3 O <sup xmlns="http://www.wiley.com/namespaces/wiley">++ , NO <sup xmlns="http://www.wiley.com/namespaces/wiley">++ , and O <sub xmlns="http://www.wiley.com/namespaces/wiley">2</sub>2 <sup xmlns="http://www.wiley.com/namespaces/wiley">++ ions</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Castada Hardy Z.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Castada Hardy Z.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Barringer Sheryl A.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Barringer Sheryl A.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wick Macdonald&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Wick Macdonald </a> <a href="/journal-foreign-26627/" target="_blank" rel="nofollow" class="tuijian_authcolor">Rapid Communications in Mass Spectrometry: RCM .</a> <span>2017</span><span>,第19期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：使用H <sub xmlns =“http://www.wiley.com/namespaces/wiley”> 3 </ sub> 3 o <sup xmlns的4-烷基支链羧酸和3-甲基吲哚的气相化学电离 =“http://www.wiley.com/namespaces/wiley”> + </ sup> +，no <sup xmlns =“http://www.wiley.com/namespaces/wiley”> + </ sup> +，和O <sub xmlns =“http://www.wiley.com/namespaces/wiley”> 2 </ sub> 2 <sup xmlns =“http://www.wiley.com/namespaces/wiley”> + </ sup> +离子</span> </p> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025814989.html">Raman study of HoFe <sub xmlns="http://www.wiley.com/namespaces/wiley">3</sub>3 (BO <sub xmlns="http://www.wiley.com/namespaces/wiley">3</sub>3 ) <sub xmlns="http://www.wiley.com/namespaces/wiley">4</sub>4 at simultaneously high pressure and high temperature: <i xmlns="http://www.wiley.com/namespaces/wiley">pp – <i xmlns="http://www.wiley.com/namespaces/wiley">TT phase diagram</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Krylov A. 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