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Assay of lovastatin containing dietary supplement by LC‐MS/MS under MRM condition

机译：在MRM条件下通过LC-MS / MS含有膳食补充剂的洛伐他汀的测定

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Abstract >Monacolin K, the active ingredient present in dietary supplement, is a nutraceutical whose health benefits have been widely documented. A fast approach for the assay of lovastatin in both forms, lactone and acid, by mass spectrometry is presented. The quantitative assay is carried out by high‐performance liquid chromatography‐tandem mass spectrometry by using the multiple reaction monitoring mode and simvastatin and pravastatin as internal standards. The accuracy values ranged from 97 to 101%; the analytical parameter values of limit of quantitation, limit of detection, recovery, and reproducibility were calculated by analyzing fortified samples, confirming the reliability of the proposed approach. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“它”> <title type =“main”>抽象</ title> > monacolin k ，膳食补充剂中存在的活性成分是一种营养保健，其健康益处已被广泛记录。提出了一种通过质谱法在两种形式，内酯和酸中进行洛伐他汀的快速方法。通过使用多重反应监测模式和辛伐他汀和普伐他汀作为内标，通过高效液相色谱 - 串联质谱法进行定量测定。精度值范围为97至101％; 通过分析强化样品来计算定量限制，检测，恢复和再现性限制的分析参数值，确认了所提出的方法的可靠性。</ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-34906/'>《Journal of mass spectrometry: JMS》</a> <b style="margin: 0 2px;">|</b><span>2018年第9期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Di Donna Leonardo&option=202" target="_blank" rel="nofollow">Di Donna Leonardo;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bartella Lucia&option=202" target="_blank" rel="nofollow">Bartella Lucia;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Napoli Anna&option=202" target="_blank" rel="nofollow">Napoli Anna;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sindona Giovanni&option=202" target="_blank" rel="nofollow">Sindona Giovanni;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mazzotti Fabio&option=202" target="_blank" rel="nofollow">Mazzotti Fabio;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Dipartimento di Chimica e Tecnologie ChimicheUniversità della CalabriaVia P. Bucci Cubo 12/C I‐87036 Arcavacata di Rende Italy;</p> <p>Dipartimento di Chimica e Tecnologie ChimicheUniversità della CalabriaVia P. Bucci Cubo 12/C I‐87036 Arcavacata di Rende Italy;</p> <p>Dipartimento di Chimica e Tecnologie ChimicheUniversità della CalabriaVia P. Bucci Cubo 12/C I‐87036 Arcavacata di Rende Italy;</p> <p>Dipartimento di Chimica e Tecnologie ChimicheUniversità della CalabriaVia P. Bucci Cubo 12/C I‐87036 Arcavacata di Rende Italy;</p> <p>Dipartimento di Chimica e Tecnologie ChimicheUniversità della CalabriaVia P. Bucci Cubo 12/C I‐87036 Arcavacata di Rende Italy;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1187.html" title="分析化学">分析化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=HPLC&option=203" rel="nofollow">HPLC;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=lovastatin&option=203" rel="nofollow">lovastatin;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=mass spectrometry&option=203" rel="nofollow">mass spectrometry;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=multiple reaction monitoring&option=203" rel="nofollow">multiple reaction monitoring;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=red yeast rice&option=203" rel="nofollow">red yeast rice;</a> </p> <div class="translation"> 机译：HPLC;Lovastatin;质谱;多重反应监测;红酵母米; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025633475.html">Assay of lovastatin containing dietary supplement by LC‐MS/MS under MRM condition</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Di Donna Leonardo&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Di Donna Leonardo,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bartella Lucia&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Bartella Lucia,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Napoli Anna&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Napoli Anna,</a> <a href="/journal-foreign-34906/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of mass spectrometry: JMS .</a> <span>2018</span><span>,第9期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：在MRM条件下通过LC-MS / MS含有膳食补充剂的洛伐他汀的测定</span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/academic-journal-foreign_analytical-bioanalytical-chemistry_thesis/020415640601.html">LC/UV/MS-MRM for the simultaneous determination of water-soluble vitamins in multi-vitamin dietary supplements</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Pei Chen&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Pei Chen,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wayne R. 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