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Microstructural and Mechanical Evaluations of Transient Liquid Phase Bonded In X-750/BNi-3/SAF 2205

机译:X-750 / BNI-3 / SAF 2205中粘接瞬态液相的微观结构和机械评价

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摘要

In this study, dissimilar joining between SAF 2205 duplex stainless steel and Inconel X-750 superalloy produced by TLP process was investigated. This process was done at temperature of 1100 degrees C for different bonding times of 1, 15, 30, 45 and 60 min. The effect of different bonding times on the microstructure and mechanical properties of the welded samples was studied. Microstructure of the samples was analyzed by optical microscopy and scanning electron microscopy equipped with energy-dispersive x-ray spectroscopy. X-ray diffraction analysis was used to determine the formed phases in the bonding area. Microhardness and shear strength tests were done to evaluate the mechanical properties of the joints. It was found that the joint area contains the gamma-Ni solid solution, eutectic compounds with intermetallic phases beside precipitated secondary phases. The gamma-Ni solid solution, BN, BCN, CrB, Ni3Si and Ni3B were the main phases in the joining area. Maximum microhardness was found in athermally solidified zone, due to the presence of hard and brittle intermetallic and boride phases. The maximum shear strength (368 MPa) was obtained for the sample with the bonding time of 45 min, due to the completion of isothermal solidification and removal of eutectic compounds.
机译:在该研究中,研究了SAF 2205双相不锈钢和INCONEL X-750超合金之间的不同接合,通过TLP工艺生产的X-750超合金。该方法在1100℃的温度下进行,对于1,15,30,45和60分钟的不同键合时间。研究了不同键合时间对焊接样品的微观结构和力学性能的影响。通过光学显微镜和扫描电子显微镜分析样品的微观结构,配备有能量分散X射线光谱。 X射线衍射分析用于确定粘合区域中的形成相。进行微硬度和剪切强度试验以评估关节的机械性能。发现接合面积含有γ-Ni固溶体,共晶化合物,沉淀的次阶旁边具有金属间相。 γ-Ni固溶体,BN,BCN,CRB,Ni3Si和Ni3B是连接区域中的主要相。由于存在硬质和脆性的金属间化和硼化阶段,在热固化区域中发现了最大微硬度。由于完成等温凝固和除去共晶化合物,获得最大剪切强度(368MPa)的键合时间为45分钟。

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