Crystal Growth and Characterization of LixLa(1-x)/3NbO3 by the Traveling Solvent Floating Zone Method

Ali Md Shahajan; Sato Nobuyoshi; Fukasawa Ikuya; Maruyama Yuki; Nagao Masanori; Watauchi Satoshi; Tanaka Isao

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Crystal Growth and Characterization of LixLa(1-x)/3NbO3 by the Traveling Solvent Floating Zone Method

机译：行进溶剂浮区法的晶晶生长和Lixla（1-x）/ 3n32的表征

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Single crystals of LixLa(1-x)/3NbO3 were grown successfully using the traveling solvent floating zone method with LaNbO4-poor and Li-rich solvents. Crack- and inclusion-free single crystals with a typical diameter and length of 6 and 35 mm, respectively, were obtained. The crystals grown under Ar flow were black in color, and become colorless and transparent upon oxygen annealing. The composition of the grown crystals was uniform with x = 0.070 +/- 0.001, which was lower that of feeds with x = 0.10 because of vaporization of the lithium component from the melt during growth. The ionic conductivity of the annealed crystal was anisotropic with sigma([100]) = 1.2 X 10(-4) S.cm(-1) and sigma([001]) = 7.4 X 10(-5) S.cm(-1).

机译：利用Lanbo4-Per和Li-Rich溶剂的行进溶剂浮区法成功地成功地生长了Lixla（1-x）/ 3nbO3的单晶。获得分别具有典型直径和长度为6和35mm的无裂缝和自由的单晶分别。在Ar流下生长的晶体颜色为黑色，并且在氧气退火时变为无色透明。生长晶体的组成具有均匀的X = 0.070 +/- 0.001，其由于锂组分在生长期间溶液而较低的X = 0.10的进料。退火晶体的离子电导率与Sigma（[100]）= 1.2×10（-4）S.cm（-1）和σ（[001]）= 7.4×10（-5）S.cm（ -1）。

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《Crystal growth & design》 |2019年第11期|共5页
作者
Ali Md Shahajan; Sato Nobuyoshi; Fukasawa Ikuya; Maruyama Yuki; Nagao Masanori; Watauchi Satoshi; Tanaka Isao;
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Univ Yamanashi Ctr Crystal Sci &

Technol 7-32 Miyamae Kofu Yamanashi Japan;

Univ Yamanashi Ctr Crystal Sci &

Technol 7-32 Miyamae Kofu Yamanashi Japan;

Univ Yamanashi Ctr Crystal Sci &

Technol 7-32 Miyamae Kofu Yamanashi Japan;

Univ Yamanashi Ctr Crystal Sci &

Technol 7-32 Miyamae Kofu Yamanashi Japan;

Univ Yamanashi Ctr Crystal Sci &

Technol 7-32 Miyamae Kofu Yamanashi Japan;

Univ Yamanashi Ctr Crystal Sci &

Technol 7-32 Miyamae Kofu Yamanashi Japan;

Univ Yamanashi Ctr Crystal Sci &

Technol 7-32 Miyamae Kofu Yamanashi Japan;

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中图分类晶体学;
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1. Crystal Growth and Characterization of LixLa(1-x)/3NbO3 by the Traveling Solvent Floating Zone Method [J] . Ali Md Shahajan, Sato Nobuyoshi, Fukasawa Ikuya, Crystal growth & design . 2019,第11期

机译：行进溶剂浮区法的晶晶生长和Lixla（1-x）/ 3n32的表征
2. Lithium-ionic conductivity of LixLa(1-x)/3NbO3 single crystals grown by the TSFZ method [J] . Solid state ionics . 2020,第期

机译：通过TSFZ法生长的Lixla（1-x）/ 3nbO3单晶的锂离子电导率
3. Crystal growth of pure and substituted low-dimensionality cuprates CuGeO_3, La_2CuO_4, SrCuO_2, Sr_2CuO_3 and Sr_14Cu_24O_41 by the floating zone and travelling solvent zone methods [J] . A. Revcolevschi, U. Ammerahl, G. Dhalenne Journal of Crystal Growth . 1999,第1期

机译：通过浮动区和移动溶剂区方法，纯净和取代的低维铜酸盐CuGeO_3，La_2CuO_4，SrCuO_2，Sr_2CuO_3和Sr_14Cu_24O_41的晶体生长
4. Growth of Phase Pure Na_(0.75)CoO_(2) Single Crystals by Traveling Solvent Floating Zone (TSFZ) Method [C] . C. Sekar, P. Kanchana, S. Paulraj, DAE Solid State Physics Symposium . 2011

机译：通过行进溶剂浮区（TSFZ）方法生长相纯NA_（0.75）COO_（2）单晶
5. Theoretical study and numerical simulations of the Hg(1-x)Cd(x)Te crystal growth by the traveling heater method [D] . Ye, Xing 1996

机译：Hg（1-x）Cd（x）Te晶体的行进加热法生长的理论研究和数值模拟
6. Floating Zone Growth and Characterization of (Ca1–xNdx)12Al14O33+6x (x ∼0.001) Single Crystals [O] . M. Mozahar Ali, Masanori Nagao, Satoshi Watauchi, 2017

机译：（Ca1-xNdx）12Al14O33 + 6x（x〜0.001）单晶
7. Growth of Bi2Sr2Ca1−xPrxCu2Oy single crystals by traveling solvent floating zone method [O] . Yeh KW 2011

机译：行进溶剂浮区法生长Bi2Sr2Ca1-xPrxCu2Oy单晶
8. Investigation of the Growth of Single Crystal Sic by the Travelling Solvent and Other Methods [R] . Das, B. N., Lamport, C. B., Mlavsky, A. I., 1968

机译：用行程溶剂和其他方法研究单晶sic的生长

Crystal Growth and Characterization of LixLa(1-x)/3NbO3 by the Traveling Solvent Floating Zone Method

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