<![CDATA[Crystal Growth and Optical Properties of Beryllium-Free Nonlinear Optical Crystal K3Ba3Li2Al4B6O20F]]>

Bingqing Zhao; Lei Bai; Bingxuan Li; Sangen Zhao; Yaoguo Shen; Xianfeng Li; Qingran Ding; Chengmin Ji; Zheshuai Lin; Junhua Luo

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3Ba₃Li₂Al₄B₆O₂₀F]]>

机译：<！[cdata [铍无线光学晶体k _{3 ba _{li _{2 _{al _{4 b _{6 O _{20 f]]>}}}}}}}

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A beryllium-free nonlinear optical (NLO) crystal K_(3)Ba_(3)Li_(2)Al_(4)B_(6)O_(20)F (KBLABF) with sizes up to 18 × 13 × 8 mm~(3) was successfully grown by the top-seeded solution growth method using LiOH-H_(3)BO_(3)–BaF_(2) flux. The key limiting factors on the crystal morphologies and sizes were carefully analyzed. Meanwhile, by using the minimum deviation technique, the refractive index dispersion was measured and fitted well by the Sellmeier equations. The results suggest that KBLABF is a negative uniaxial crystal with moderate birefringence of 0.06050–0.06834 at a wavelength range from 363 to 852.1 nm. Furthermore, the type-I phase matching range for fundamental (second harmonic) light is down to 486 (243 nm) in theory, which indicates that KBLABF crystal could achieve 532 and 266 nm light generation by direct second-harmonic generation. As compared with the famous NLO crystals β-BaB_(2)O_(4) and CsLiB_(6)O_(10), KBLABF crystal exhibits a smaller walk-off angle and larger acceptance angle at the wavelength of 532 nm while having a comparable short absorption edge, sufficient birefringence, and moderate NLO response. Furthermore, in contrast to highly hygroscopic CsLiB_(6)O_(10), it is nonhygroscopic. These attributes make KBLABF a promising candidate for practical applications in UV light generation.

机译：无铍非线性光学（NLO）晶体K_（3）BA_（3）LI_（2）AL_（4）B_（6）O_（20）F（kblabf）尺寸高达18×13×8 mm〜（ 3）通过使用LiOH-H_（3）BO_（3）-BAF_（2）通量的瓶盖溶液生长方法成功生长。仔细分析了晶体形态和尺寸的关键限制因素。同时，通过使用最小偏差技术，通过销售方程测量折射率分散体并装配良好。结果表明，Kblabf是负单轴晶体，其波长范围为0.06050-0.06834的中等双折射从363至852.1nm。此外，关于基本（二次谐波）光的I相位匹配范围在理论下降至486（243nm），这表明Kblabf晶体可以通过直接的二次谐波产生来实现532和266nm光产生。与着名的NLO晶体β-BAB_（2）O_（4）和CSLIB_（6）O_（10）相比，Kblabf晶体在532nm波长的同时表现出较小的步道角度和更大的接受角，同时具有可比较短吸收边缘，足够的双折射和中等NLO反应。此外，与高吸湿性的CsLib_（6）O_（10）相反，它是非显眼的。这些属性使KBLABF成为UV光生成中实际应用的有希望的候选者。

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《Crystal growth & design》 |2018年第2期|共5页
作者
Bingqing Zhao; Lei Bai; Bingxuan Li; Sangen Zhao; Yaoguo Shen; Xianfeng Li; Qingran Ding; Chengmin Ji; Zheshuai Lin; Junhua Luo;
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State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter Chinese Academy of Sciences Fuzhou Fujian 350002 China;

Beijing Center for Crystal R&

D Key Lab of Functional Crystals and Laser Technology of Chinese Academy of Sciences Technical Institute of Physics and Chemistry Chinese Academy of Sciences Beijing 100190 China;

Beijing Center for Crystal R&

D Key Lab of Functional Crystals and Laser Technology of Chinese Academy of Sciences Technical Institute of Physics and Chemistry Chinese Academy of Sciences Beijing 100190 China;

State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter Chinese Academy of Sciences Fuzhou Fujian 350002 China;

State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter Chinese Academy of Sciences Fuzhou Fujian 350002 China;

State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter Chinese Academy of Sciences Fuzhou Fujian 350002 China;

State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter Chinese Academy of Sciences Fuzhou Fujian 350002 China;

State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter Chinese Academy of Sciences Fuzhou Fujian 350002 China;

Beijing Center for Crystal R&

D Key Lab of Functional Crystals and Laser Technology of Chinese Academy of Sciences Technical Institute of Physics and Chemistry Chinese Academy of Sciences Beijing 100190 China;

State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter Chinese Academy of Sciences Fuzhou Fujian 350002 China;

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