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首页> 外文期刊>Crystal growth & design >Experimental Characterization and Mathematical Modeling of Breakage of Needle-like Crystals in a Continuous Rotor-Stator Wet Mill
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Experimental Characterization and Mathematical Modeling of Breakage of Needle-like Crystals in a Continuous Rotor-Stator Wet Mill

机译:连续转子定子湿磨机中针状晶体破损的实验表征及数学建模

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摘要

In this work, thorough experimental characterization and theoretical investigation for the quantitative description of the breakage of needlelike crystals of beta L-glutamic acid in a continuous rotor-stator wet mill are performed. The constitutive equations of the newly developed model rely on the physics of the phenomena occurring at the single crystal and at the process scale. The fundamental equations consider not only the operating conditions adopted for the grinding device but also the morphology of the crystals. First, a comprehensive experimental campaign is performed to investigate the effect of the different operating conditions, namely, the suspension density, the rotor speed, and the residence time in the grinding chamber, on the product properties, in particular, the average sizes and the particle size and shape distribution. Measurements are collected using an in-house developed double-camera stereoscopic measurement device, the mu-DISCO, capable of quantitatively measuring the particle size and shape distribution. The data collected shed light on aspects previously hardly accessible, providing a set of robust quantitative information for a thorough experimental characterization of a continuous milling process. Furthermore, these data can be used to estimate the kinetic parameters and to obtain a model, which is able to quantitatively predict the product properties.
机译:在这项工作中,进行了彻底的实验表征和对连续转子 - 定子湿磨机中β1-谷氨酸的β晶体破裂的裂缝的定量描述的彻底实验表征和理论研究。新开发模型的本构方程依赖于在单晶和过程规模处发生的现象的物理学。基本方程不仅考虑磨削装置采用的操作条件,还考虑晶体的形态。首先,进行全面的实验活动,以研究不同的操作条件,即悬架密度,转子速度和在研磨室中的停留时间的效果,特别是平均尺寸和粒度和形状分布。使用内部开发的双摄像机立体测量装置,MU-DICKO收集测量,能够定量测量粒度和形状分布。数据收集了先前几乎无法访问的方面的缩小光,提供了一组稳健的定量信息,用于彻底实验表征连续铣削过程。此外,这些数据可用于估计动力学参数并获得能够定量预测产品性质的模型。

著录项

  • 来源
    《Crystal growth & design》 |2018年第10期|共16页
  • 作者单位

    Swiss Fed Inst Technol Inst Proc Engn CH-8092 Zurich Switzerland;

    Swiss Fed Inst Technol Inst Proc Engn CH-8092 Zurich Switzerland;

  • 收录信息
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 晶体学;
  • 关键词

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