Highly Interpenetrated Robust Microporous Hydrogen-Bonded Organic Framework for Gas Separation

Yang Wei; Wang Jiawei; Wang Hailong; Bao Zongbi; Zhao John Cong-Gui; Chen Banglin

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Highly Interpenetrated Robust Microporous Hydrogen-Bonded Organic Framework for Gas Separation

机译：高度互连的气体分离的鲁棒微孔氢键有机框架

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A hydrogen-bonded organic framework (HOF), HOF-11, has been successfully prepared by the slow diffusion of hexane into a tetrahydrofuran solution of tris(4-carboxyphenyl)amine (TCPA). HOF-11 has been characterized by single-crystal and powder X-ray diffraction analysis, which is composed of TCPA ligands connected by the intermolecular hydrogen-bonding interactions in the carboxylic group dimer, showing 11-fold interpenetrated three-dimensional hydrogen-bonded networks in a (10,3)-b topology with the pore size of 6.2 x 6.8 angstrom(2). The permanent porosity of degassed HOF was demonstrated by virtue of the CO2 sorption and selective gas adsorption.

机译：通过己烷缓慢扩散成Tris（4-羧基苯基）胺（TCPA）的四氢呋喃溶液，成功地制备了氢键合有机骨架（HOF）HOF-11。 HOF-11的特征在于单晶和粉末X射线衍射分析，其由通过羧基二聚体中的分子间氢键相互作用连接的TCPA配体组成，显示11倍互连的三维氢键网络在（10,3）-B拓扑中，孔径为6.2 x 6.8埃（2）。通过CO 2吸附和选择性气体吸附来证明脱气HOF的永久孔隙率。

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来源
《Crystal growth & design》 |2017年第11期|共6页
作者
Yang Wei; Wang Jiawei; Wang Hailong; Bao Zongbi; Zhao John Cong-Gui; Chen Banglin;
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作者单位

Univ Texas San Antonio Dept Chem San Antonio TX 78249 USA;

Zhejiang Univ Coll Chem &

Biol Engn Key Lab Biomass Chem Engn Minist Educ Hangzhou 310027 Zhejiang Peoples R China;

Univ Texas San Antonio Dept Chem San Antonio TX 78249 USA;

Univ Texas San Antonio Dept Chem San Antonio TX 78249 USA;

Univ Texas San Antonio Dept Chem San Antonio TX 78249 USA;

Univ Texas San Antonio Dept Chem San Antonio TX 78249 USA;

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原文格式 PDF
正文语种 eng
中图分类晶体学;
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1. Highly Interpenetrated Robust Microporous Hydrogen-Bonded Organic Framework for Gas Separation [J] . Yang Wei, Wang Jiawei, Wang Hailong, Crystal growth & design . 2017,第11期

机译：高度互连的气体分离的鲁棒微孔氢键有机框架
2. Robust Microporous Porphyrin-Based Hydrogen-Bonded Organic Framework for Highly Selective Separation of C-2 Hydrocarbons versus Methane [J] . Yin Qi, Lu Jian, Li Hong-Fang, Crystal growth & design . 2019,第7期

机译：基于鲁棒的微孔卟啉基氢键有机框架，用于高选择性分离C-2烃与甲烷
3. Selective Ethane/Ethylene Separation in a Robust Microporous Hydrogen-Bonded Organic Framework [J] . Xu Zhang, Libo Li, Jia-Xin Wang, Journal of the American Chemical Society . 2020,第1期

机译：鲁棒的微孔氢键键合有机骨架中的选择性乙烷/乙烯分离
4. A MICROPOROUS HYDROGEN-BONDED ORGANIC FRAMEWORK FOR HIGHLY SELECTIVE C2H2/C2H4 SEPARATION AT AMBIENT TEMPERATURE [C] . Peng Li, Banglin Chen ACS National Meeting and Exhibition . 2014

机译：用于在环境温度下的高选择性C 2 H 2 / C 2 H 4分离的微孔氢键有机骨架
5. Small gases and hydrocarbon adsorption and separation in Microporous Metal Organic Frameworks (MMOFs). [D] . Wu, Haohan. 2013

机译：微孔金属有机骨架（MMOF）中的小气体和碳氢化合物吸附和分离。
6. Impact of the Preparation Procedure on the Performance of the Microporous HKUST-1 Metal-Organic Framework in the Liquid-Phase Separation of Aromatic Compounds [O] . Vera I. Isaeva, Bulat R. Saifutdinov, Vladimir V. Chernyshev, 2020

机译：制备工艺对芳香化合物液相分离中微孔HKUST-1金属有机骨架性能的影响
7. A microporous six-fold interpenetrated hydrogen-bonded organic framework for highly selective separation of C2H4/C2H6 [O] . Li, P., He, Y., Arman, H.D., 2014

机译：微孔六折互穿氢键有机骨架，可高度选择性地分离C2H4 / C2H6

Highly Interpenetrated Robust Microporous Hydrogen-Bonded Organic Framework for Gas Separation

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