Development of Measurement Tools for High-Throughput Experiments of Synchrotron Radiation XRD and XAFS on Powder Libraries

Kenjiro  Fujimoto; Akihisa  Aimi; Shingo  Maruyama

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Development of Measurement Tools for High-Throughput Experiments of Synchrotron Radiation XRD and XAFS on Powder Libraries

机译：Synchrotron辐射XRD和XAFS在粉末库中的高通量实验的测量工具的研制

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We propose to minimize the sampling time for high-throughput measurements of powder X-ray diffraction (XRD) and X-ray absorption fine structure (XAFS) in synchrotron radiation. The conventional synchrotron radiation powder X-ray diffraction method requires filling of a capillary tube, but a structure-refining diffraction pattern could be obtained by transferring the crushed powder to a tape and rotating the cassette-tape tool by ±5° around the sample position. XAFS spectra could also be measured with the sample attached to the tape. The time required for sample preparation was greatly reduced, which made high-throughput experiments with powders in synchrotron radiation experiments more accessible.

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来源
《ACS combinatorial science》 |2020年第12期|共4页
作者
Kenjiro Fujimoto; Akihisa Aimi; Shingo Maruyama;
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作者单位

Department of Pure and Applied Chemistry Faculty of Science and Technology Tokyo University of Science;

Department of Pure and Applied Chemistry Faculty of Science and Technology Tokyo University of Science;

Department of Applied Chemistry School of Engineering Tohoku University;

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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
synchrotron; powder; powder X-ray diffraction; X-ray absorption fine structure;

机译：同步;粉末;粉末X射线衍射;X射线吸收细结构;

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专利

1. Infrared synchrotron radiation spectroscopy and microspectroscopy: new tools for interdisciplinary applications [J] . 核技术（英文版） . 2003,第002期
2. Bunch-by-bunch beam size measurement during injection at Shanghai Synchrotron Radiation Facility [J] . Han-Jiao Chen, Jie Chen, Bo Gao, 核技术（英文版） . 2018,第006期
3. Transverse beam size measurement system using visible synchrotron radiation at HLS Ⅱ [J] . Kai Tang, Bao-Gen Sun, Yong-Liang Yang, 中国物理C（英文版） . 2016,第009期
4. Quantitative Measurement of the Proportions of High-Order Harmonics for the 4B7B Soft-X-Ray Source at Beijing Synchrotron Radiation Facility [J] . ZHU Tuo, SHANG Wanli, ZHANG Wenhai, 等离子体科学和技术（英文版） . 2013,第012期
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6. Clay pigment structure characterisation as a guide for provenance determination—a comparison between laboratory powder micro-XRD and synchrotron radiation XRD [J] . Silvie Švarcová, Petr Bezdička, David Hradil, Analytical and Bioanalytical Chemistry . 2011,第1期

机译：粘土颜料结构表征作为物源确定的指南-实验室粉末微XRD与同步辐射XRD之间的比较
7. Clay pigment structure characterisation as a guide for provenance determination-a comparison between laboratory powder micro-XRD and synchrotron radiation XRD [J] . ?varcová S., Bezdi?ka P., Hradil D., Analytical and bioanalytical chemistry . 2011,第1期

机译：粘土颜料结构表征作为物源确定的指南-实验室粉末微XRD与同步辐射XRD的比较
8. Development of in situ cell for simultaneous XAFS/XRD measurements at high temperatures [J] . Kimijima Kenichi, Watanabe Toshiki, Takeichi Yasuo, Radiation Physics and Chemistry . 2020,第1期

机译：在高温下同时XAFS / XRD测量的原位小区的开发
9. In Situ Synchrotron Radiation XRD and XAFS Measurements of Multilayer All-Solid-State Lithium-Ion Batteries Using Li_2CoP_2O_7 as a Positive Electrode Material [C] . Chihiro Yamamoto, Shuichi Doi, Masanori Nakanishi, Pacific Rim Meeting on Electrochemical and Solid-State Science . 2020

机译：原位同步辐射XRD和XAFS使用Li_2cop_2O_7作为正极材料的多层全固态锂离子电池的测量
10. Synchrotron radiation from laser-electron interactions: Measurement and modeling. [D] . Semenov, Vladimir Alexandrovich. 2009

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11. Development of optical choppers for time-resolved measurements at soft X-ray synchrotron radiation beamlines [O] . Hitoshi Osawa, Takuo Ohkochi, Masami Fujisawa, -1

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12. Development of Measurement Tools for High-Throughput Experiments of Synchrotron Radiation XRD and XAFS on Powder Libraries [O] . -1

机译：在粉末库中同步辐射XRD和XAFS的高通量试验测量工具的研制
13. Synchrotron Radiation XRD Analysis of Indialite in Y-82094 Ungrouped Carbonaceous Chondrite. [R] . Mikouchi, T., Hagiya, K., Sawa, N., 2016

机译：Y-82094未分解碳质球粒陨石中Indialite的同步辐射X射线衍射分析。

Development of Measurement Tools for High-Throughput Experiments of Synchrotron Radiation XRD and XAFS on Powder Libraries

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