Voltammetric Determination of an Anti-rheumatoid Drug Acemetacin on Graphite Flake Paste Electrode and Glassy Carbon Electrode

Festinger Natalia; Smarzewska Sylwia; Mirceski Valentin; Ciesielski Witold

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Voltammetric Determination of an Anti-rheumatoid Drug Acemetacin on Graphite Flake Paste Electrode and Glassy Carbon Electrode

机译：伏安法测定石墨薄浆浆料电极上抗类风湿药物血清酸和玻碳电极

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In this study, a simple and sensitive square wave voltammetric procedure has been developed for the determination of acemetacin (ACM) at graphite flake paste electrode (GFPE) and glassy carbon electrode (GCE). Under optimized conditions, the dependence of ACM peak current on its concentration showed wide linear range: 0.03-1.0 mu mol L(-1)and 0.7-15.0 mu mol L(-1)at GFPE and GCE, respectively. The developed method was successfully applied for the determination of ACM in pharmaceuticals and spiked urine with satisfying recoveries. The electrochemical oxidation of ACM is an irreversible process controlled by mixed nature of the mass transfer process.

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来源
《Electroanalysis》 |2021年第2期|共9页
作者
Festinger Natalia; Smarzewska Sylwia; Mirceski Valentin; Ciesielski Witold;
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作者单位

Univ Lodz Fac Chem Dept Inorgan &

Analyt Chem 12 Tamka St PL-91403 Lodz Poland;

Univ Lodz Fac Chem Dept Inorgan &

Analyt Chem 12 Tamka St PL-91403 Lodz Poland;

Ss Cyril &

Methodius Univ Fac Nat Sci &

Math Inst Chem 3 Arhimedova St Skopje 1000 North Macedonia;

Univ Lodz Fac Chem Dept Inorgan &

Analyt Chem 12 Tamka St PL-91403 Lodz Poland;

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原文格式 PDF
正文语种 eng
中图分类电化学、电解、磁化学;
关键词
acemetacin; electrochemistry; glassy carbon electrode; graphite flake paste electrode; voltammetry;

机译：Acemetacin;电化学;玻璃碳电极;石墨片浆料电极;伏安法;

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Voltammetric Determination of an Anti-rheumatoid Drug Acemetacin on Graphite Flake Paste Electrode and Glassy Carbon Electrode

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