A Hyper-conjugated Structure: The Research into the Picryl Chloride Functionalized 1-Picrylamino-tetrazol-5-one

Zhang Gu-Dan; Wang Zhen; Yin Xin; Zhang Jian-Guo

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A Hyper-conjugated Structure: The Research into the Picryl Chloride Functionalized 1-Picrylamino-tetrazol-5-one

机译：超缀合的结构：研究磷灰酰氯官能化1-Picrylamino-Tetrazol-5-one

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摘要

A hyper conjugated structure, picryl chloride functionalized 1-picrylamino-tetrazol-5-one, was synthesized by a nucleophilic substitution reaction. The single crystals of 1-picrylamino-tetrazol-5-one were cultured and determined by X-ray single-crystal diffractometer. The thermal behavior was investigated by differential scanning calorimetry (DSC) and thermogravimetry-derivative thermogravimetry (TG-DTG) technologies. Additionally, the sensitivities towards friction and impact were tested. The results show that the hyper conjugated structure adopts a - stacking, besides, many strong interactions such as nitro- and hydrogen bonding interactions were observed. All of them together make a contribution to its enhanced thermal stability and reduced sensitivities. 1-Picrylamino-tetrazol-5-one turns out to be a representative of hyper conjugated structures in energetic materials, and may further strengthen the functionalization of picryl chloride with energetic tetrazoles.

机译：通过亲核取代反应合成了一种超共轭结构，苦味酸氯官能化1-苦味酸氨基四唑-5-酮。对1-吡啶氨基四唑-5-酮的单晶进行培养，并用X射线单晶衍射仪进行测定。用差示扫描量热法（DSC）和热重导数热重法（TG-DTG）研究了其热行为。此外，还测试了对摩擦和冲击的敏感性。结果表明，超共轭结构采用a-堆积，并且观察到许多强相互作用，如硝基和氢键相互作用。所有这些都有助于提高其热稳定性和降低灵敏度。1-苦味酸氨基四唑-5-酮是含能材料中超共轭结构的代表，可能进一步加强苦味酸氯化物与含能四唑的功能化。

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来源
《Zeitschrift fur Anorganische und Allgemeine Chemie》 |2018年第13期|共4页
作者
Zhang Gu-Dan; Wang Zhen; Yin Xin; Zhang Jian-Guo;
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作者单位

Beijing Inst Technol State Key Lab Explos Sci &

Technol Beijing 100081 Peoples R China;

Beijing Inst Technol State Key Lab Explos Sci &

Technol Beijing 100081 Peoples R China;

Beijing Inst Technol State Key Lab Explos Sci &

Technol Beijing 100081 Peoples R China;

Beijing Inst Technol State Key Lab Explos Sci &

Technol Beijing 100081 Peoples R China;

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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
1-Picrylamino-tetrazol-5-one; 1-Amino-tetrazol-5-one (ATO); Picryl chloride (PiCl); Hyper conjugated structure; Thermal stability;

机译：1-PICRYLAMINO-四唑-5-one;1-氨基 - 四唑-5-ONE（ATO）;Picryl氯化物（PICL）;超缀合结构;热稳定性;

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8. THE CRYSTAL STRUCTURE DETERMINATIONS OF PENTAMERIC CUPRIC-CHLORIDE DI-ISOPROPANOL, DYSPROSIUM-CHLORIDE HEXAHYDRATE AND SILVER PERCHLORATE 4L(L = 4-METHYL-3,5,8-TRIUXA-1-PHOSPHA-BICYCLO(2.2.2)OCTANE). [D] . URGO, JOSEF VENDAL, JR. 1967

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11. Synthesis of picryl chloride. [R] . Hayes, D. V., Honea, F. I. 1970

机译：木瓜酰氯的合成。

A Hyper-conjugated Structure: The Research into the Picryl Chloride Functionalized 1-Picrylamino-tetrazol-5-one

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