Synthesis of picryl chloride.

机译：木瓜酰氯的合成。

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A total of six pilot-scale batches of picryl chloride were made. These included three 5-kg batches and three 10-kg batches. The three 5-kg batches were made to investigate the problems encountered with actual production and materials handling. The three 10-kg batches were made to study the process parameters and the yield problems originally encountered with the 5-kg batches. The yields on the 5-kg batches ranged from 40 to 60% of approximately 50% purity. The yields on the 10-kg batches were 80, 86 and 91% in chronological order. The purities were 95, 99+ and 99+% respectively.

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作者
Hayes, D. V.; Honea, F. I.;
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年度 1970
页码 1-22
总页数 22
原文格式 PDF
正文语种 eng
中图分类工业技术;
关键词
Chemical explosives; Synthesis(Chemistry); Chemical Preparation; Chemical Reaction Yield; Nitrophenol; Organic Chlorine Compounds; Picryl chloride; EDB/450100;

机译：化学炸药;合成（化学）;化学制备;化学反应产率;硝基酚;有机氯化合物;苦基氯; EDB / 450100;

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1. Protective involvement of nitric oxide in the liver injury induced by delayed-type hypersensitivity to picryl chloride. [J] . Cao J, Xu Q, Koda A Inflammation research: Official journal of the European Histamine Research Society . 2000,第11期

机译：一氧化氮对氯化苦的迟发型超敏反应引起的肝损伤的保护作用。
2. Role of Th1 and Th2 cytokines in regulating the liver injury induced by delayed-type hypersensitivity to picryl chloride. [J] . Xu Q, Cao J, Wu F, Liver . 1999,第6期

机译：Th1和Th2细胞因子在调节对氯化苦的迟发型超敏反应诱导的肝损伤中的作用。
3. LEA-1/ICAM-1 interaction is essentially involved in the pathogenesis of delayed-type hypersensitivity-induced liver injury to picryl chloride. [J] . Xu Q, Jiang J, Cao J, Life sciences . 1998,第15期

机译：LEA-1 / ICAM-1相互作用本质上参与了迟发型超敏反应引起的对氯化聚吡啶的肝损伤的发病机理。
4. A fast and feasible synthesis for picryl bromide [C] . Dominik E. Dosch, Thomas M. Klapoetke Seminar on new trends in research of energetic materials . 2018

机译：一种快速可行的溴化吡咯合成方法
5. The formation of polychlorinated dibenzo-p-dioxins/dibenzofurans (PCDD/F) via the de novo synthesis in the catalytic extraction process (CEP) and the role of iron chloride. [D] . Ryan, Shawn Patrick. 2001

机译：在催化萃取过程（CEP）中通过从头合成和氯化铁的作用形成多氯代二苯并-对-二恶英/二苯并呋喃（PCDD / F）。
6. T suppressor cells and suppressor factor which act at the efferent stage of the contact sensitivity skin reaction: their production by mice injected with water-soluble, chemically reactive derivatives of oxazolone and picryl chloride. [O] . G L Asherson, M Zembala 2014

机译：T抑制细胞和抑制因子，在接触敏感性皮肤反应的后继阶段起作用：它们是由注射了恶唑酮和氯化三甲基吡啶的水溶性，化学反应性衍生物的小鼠生产的。
7. Synthesis of Polyamides by Direct Polycondensation with Picryl Chloride. II. Reaction Conditions and Mechanism [O] . Hozumi Tanaka, Guo-chuang Wu, Yuki Iwanaga, 1982

机译：用普通氯化物直接缩聚合成聚酰胺。 II。反应条件和机制
8. 2-Picryl-5-Nitrotetrazole: Synthesis and Explosive Properties [R] . Spear, R. J., Elischer, P. P. 1982

机译：2-吡啶-5-硝基四唑：合成和爆炸性质

Synthesis of picryl chloride.

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