Syntheses, spectroscopic studies, crystal structure and complexation reactions of N- (2 or 4-hydroxylphenyl) benzaldimine

Rajib Lal De; Mahuya Mandal; Lovely Roy

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Syntheses, spectroscopic studies, crystal structure and complexation reactions of N- (2 or 4-hydroxylphenyl) benzaldimine

机译：N-（2或4-羟基苯基）苯甲二胺的合成，光谱研究，晶体结构和络合反应

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Two monobasic bidentate Schiff base ligands (SBH) derived from the condensation reaction between benzaldehyde and 2-aminophenol (BENOPH) or 4-aminophenol (BENPAPH) have been subjected to complexation -reactions stabilising the bis-ligated complexes M~(II)(SB)2 (M~(II)=Cu, Ni, Co and Zn) where aminophenolic (-OH) groups participate in the complexation reaction. The newly synthesized Schiff bases and their complexes are characterized by elemental analysis, magnetic, spectroscopic and electrochemical studies. Crystal structure studies performed on BENPAPH show it to crystallize in the monoclinic form, space group P2_1/c; Z=4 with a, 6.500(7); b, 14.885(3); c, 10.852(2) A and β 91.489(12)°.

机译：苯甲醛与2-氨基苯酚（BENOPH）或4-氨基苯酚（BENPAPH）缩合反应得到的两个一元二齿Schiff碱配体（SBH）已进行了络合反应，以稳定双连接的配合物M〜（II）（SB ）2（M〜（II）= Cu，Ni，Co和Zn），其中氨基酚（-OH）基团参与络合反应。新合成的席夫碱及其配合物的特征在于元素分析，磁性，光谱学和电化学研究。在BENPAPH上进行的晶体结构研究表明，它以单斜晶型空间群P2_1 / c结晶。 Z = 4，a为6.500（7）; b，14.885（3）; c，10.852（2）A和β91.489（12）°。

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《Indian Journal of Chemistry, Section A. Inorganic, Physical, Theoretical & Analytical》 |2008年第2期|共7页
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Rajib Lal De; Mahuya Mandal; Lovely Roy;
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Syntheses, spectroscopic studies, crystal structure and complexation reactions of N- (2 or 4-hydroxylphenyl) benzaldimine

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