Synthesis of nanocrystalline Ni_2B via a solvo-thermal route

Xin Feng; Yu-Jun Bai; Bo Lu; Yong-Rui Zhao; Jie Yang; Jie-Ru Chi

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Synthesis of nanocrystalline Ni_2B via a solvo-thermal route

机译：溶剂热合成纳米晶Ni_2B

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Nickel boride (Ni_2B) nanocrystals were success fully synthesized via the reaction of NiCl_2 and NaBH_4 at 420 deg C with benzene as solvent.The yield is about 60%.The crystals were characterized by X-ray powder diffraction (XRD),transmission electron microscopy (TEM) and X-ray photoelectron spectra (XPS).Highly crystallized Ni_2B with an average size of 20 nm was obtained.

机译：通过NiCl_2和NaBH_4在420℃下以苯为溶剂反应成功合成了硼化镍（Ni_2B）纳米晶体，收率约为60％。通过X射线粉末衍射（XRD），透射电子显微镜对晶体进行了表征。（TEM）和X射线光电子能谱（XPS）。获得了平均粒径为20 nm的高度结晶的Ni_2B。

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来源
《Inorganic Chemistry Communications》 |2004年第2期|共3页
作者
Xin Feng; Yu-Jun Bai; Bo Lu; Yong-Rui Zhao; Jie Yang; Jie-Ru Chi;
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正文语种 eng
中图分类无机化学;
关键词
nickel boride; solvo-thermal route; Xray powder diffraction; transmission electron microscopy; X-ray ophotoelectron spectra;

机译：硼化镍;溶剂热路径;X射线粉末衍射;透射电镜;X射线光电子能谱;

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1. Synthesis of nanocrystalline Ni_2B via a solvo-thermal route [J] . Xin Feng, Yu-Jun Bai, Bo Lu, Inorganic Chemistry Communications . 2004,第2期

机译：溶剂热合成纳米晶Ni_2B
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Synthesis of nanocrystalline Ni_2B via a solvo-thermal route

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