Synthesis of alpha-tellurium dioxide nanorods from elemental tellurium by laser ablation

Zhi-Yuan Jiang; Zhao-Xiong Xie; Xian-Hua Zhang; Su-Yuan Xie; Rong-Bin Huang; Lan-Sun Zheng

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Synthesis of alpha-tellurium dioxide nanorods from elemental tellurium by laser ablation

机译：激光烧蚀法从元素碲合成α-二氧化碲纳米棒

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Elemental tellurium was evalporated by laser ablation,the vapor of which was condensed and deposited on the surface of the heated glass surface and then formed alpha-tellurium dioxide nanorods with uniformly size distribution by oxidation in the chamber with hot air atmosphere.TEM images and Electron diffraction (ED) pattern confirm the crystallinity of alpha-phase tellurium dioxide.The formation process of the nanorods involves a vapor-liquid-solid (VLS) following a chemical oxidation in the hot air atmosphere,in which the low melting point tellurium serves as a liquid-forming reagent.

机译：通过激光烧蚀散发元素碲，将其蒸气冷凝并沉积在加热的玻璃表面上，然后通过在热空气气氛中进行氧化而形成尺寸均匀分布的α-二氧化碲纳米棒。TEM图像和电子衍射图谱（ED）证实了α相二氧化碲的结晶性。纳米棒的形成过程涉及在热空气中进行化学氧化后的气液固（VLS），其中低熔点碲为液体形成试剂。

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来源
《Inorganic Chemistry Communications》 |2004年第2期|共3页
作者
Zhi-Yuan Jiang; Zhao-Xiong Xie; Xian-Hua Zhang; Su-Yuan Xie; Rong-Bin Huang; Lan-Sun Zheng;
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正文语种 eng
中图分类无机化学;
关键词
nanorod; telluirum dioxide; laser ablation;

机译：纳米棒;二氧化碲;激光烧蚀;

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专利

1. Synthesis of alpha-tellurium dioxide nanorods from elemental tellurium by laser ablation [J] . Zhi-Yuan Jiang, Zhao-Xiong Xie, Xian-Hua Zhang, Inorganic Chemistry Communications . 2004,第2期

机译：激光烧蚀法从元素碲合成α-二氧化碲纳米棒
2. Laser ablation synthesis of new gold tellurides using tellurium and nanogold as precursors. Laser desorption ionisation time-of-flight mass spectrometry [J] . Katarína ?vihlová, Lubomír Proke?, Dana Skácelová, Rapid Communications in Mass Spectrometry: RCM . 2013,第14期

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3. Laser desorption/ionization and laser ablation synthesis of new selenium oxide compounds from selenium(IV) dioxide [J] . Spalt Z, Pena-Mendez EM, Alberti M, Rapid Communications in Mass Spectrometry: RCM . 2006,第6期

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4. Elemental mapping of polychrome ancient glasses by laser ablation ICP-MS and EPMA-WDS: a new approach to the study of elemental distribution and correlation. [C] . Panighello S., ?elih V.S., van Elteren J.T., International Conference on Integrated Approaches to the Study of Historical Glass . 2012

机译：激光消融ICP-MS和EPMA-WDS多彩古眼镜的元素映射：一种新的元素分布与相关性的研究。
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机译：钴（II）-二氧化钛纳米棒的合成，表征和光催化活性，以及用于自清洁应用的二氧化钛纳米颗粒/纳诺德复合膜的电泳沉积。
6. Synthesis of Supported Heterogeneous Catalysts by Laser Ablation of Metallic Palladium in Supercritical Carbon Dioxide Medium [O] . Oleg Parenago, Alexey Rybaltovsky, Evgeniy Epifanov, 2020

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7. Elemental Analysis of Printing Inks Using Tandem Laser- Induced Breakdown Spectroscopy and Laser Ablation Inductively Coupled Plasma Mass Spectrometry [O] . Subedi Kiran 2015

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8. Elemental Analysis of the JSC Mars-1 Soil Simulant using Laser Ablation and Magnetic Separation. [R] . Nasab, Ahab S. 2005

机译：利用激光烧蚀和磁分离对JsC mars-1土壤模拟物的元素分析。

Synthesis of alpha-tellurium dioxide nanorods from elemental tellurium by laser ablation

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