Preparation and structural characterization of a dicopper prehelicate

Edwin C.Constable; Catherine E.Housecroft; Markus Neuburger; Silvia Schaffner; Ellen J.Shardlow

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Preparation and structural characterization of a dicopper prehelicate

机译：Dicopper prehelicate的制备和结构表征

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In the reaction of 4'-(4-ethynylphenyl)-2,2':6',2"-terpyridine(3)with trans-[PtI_2(PEt_3)_2] and CuI,ligand 3 scavenges Cu(I)and forms [Cu_2(PPh_3)_2(mu-I)(mu-3)]I,structural characterization of which shows that ligand 3 adopts a helical twist that parallels that found in related double helicates.

机译：在4'-（4-乙炔基苯基）-2,2'：6'，2“-吡啶（3）与反式[PtI_2（PEt_3）_2]和CuI的反应中，配体3清除Cu（I）并形成[Cu_2（PPh_3）_2（mu-I）（mu-3）] I的结构表征表明，配体3具有与相关双螺旋相同的螺旋扭曲。

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《Inorganic Chemistry Communications》 |2005年第8期|共3页
作者
Edwin C.Constable; Catherine E.Housecroft; Markus Neuburger; Silvia Schaffner; Ellen J.Shardlow;
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正文语种 eng
中图分类无机化学;
关键词
Copper(I); Helicate; Oligopyridine ligand; Alkyne; Dinuclear;

机译：铜（I）;螺盐;寡吡啶配体;炔;双核;

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Preparation and structural characterization of a dicopper prehelicate

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