Synthesis, crystal structure and characterization of hexakis2-methoxy-4-formylphenoxycyclotriphosphazene

Tumer  Y; Bati  H; Caliskan  NYuksektepe  CBuyukgungor  O

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Synthesis, crystal structure and characterization of hexakis2-methoxy-4-formylphenoxycyclotriphosphazene

机译：六2-甲氧基-4-甲酰基苯氧基环三磷腈的合成、晶体结构及表征

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摘要

The new cyclotriphosphazene derivative N3P3(OC6H3OCH3COH)(6) (1) was synthesized from hexachlorocyclotriphosphazene, N3P3Cl6, and 4-hydroxy-3-methoxybenzaldehyde in acetonitrile in the presence of K2CO3. The structure of 1 was verified by means of elemental analysis, IR, H-1 NMR, C-13 NMR, P-31 NMR spectra, thermal analysis and X-ray diffraction.

机译：以六氯环三磷腈、N3P3Cl6和4-羟基-3-甲氧基苯甲醛为乙腈，在K2CO3存在下合成了新的环三磷腈衍生物N3P3（OC6H3OCH3COH）（6）（1）。通过元素分析、红外光谱、H-1核磁共振、C-13核磁共振、P-31核磁共振光谱、热分析和X射线衍射等手段验证了1的结构。

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来源
《Zeitschrift fur Anorganische und Allgemeine Chemie》 |2008年第3期|597-599|共3页
作者
Tumer Y; Bati H; Caliskan NYuksektepe CBuyukgungor O;
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作者单位

Ondokuz Mayis Univ, Dept Chem, Fac Arts & Sci, TR-55139 Kurupelit, Turkey;

Ondokuz Mayis Univ, Dept Phys, Fac Arts & Sci, TR-55139 Kurupelit, Turkey;

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正文语种英语
中图分类化学;
关键词
hexachlorocyclotriphosphazene; crystal structure; 4-hydroxy-3-metlioxy-benzaldehyde; thermal analysis; CYCLOTRIPHOSPHAZENES; PHOSPHAZENES; COORDINATION;

机译：六氯环三磷腈;晶体结构;4-羟基-3-甲基苯甲醛;热分析;环三磷杂素;磷腈;协调;

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Synthesis, crystal structure and characterization of hexakis2-methoxy-4-formylphenoxycyclotriphosphazene

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