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Structural, microstructural and magnetic properties of 1% Fe-doped ZnO powder nanostructures prepared by mechanical alloying

机译:机械合金化制备的1%Fe掺杂ZnO粉末纳米结构的结构,微观结构和磁性

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摘要

ZnO powder nanoparticles were doped with iron (mixing produced by mechanical alloying). Their structure, microstructure and magnetic properties were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM) and vibrating sample magnetometry (VSM). ZnO starting pure powder exhibits a hexagonal crystal structure with space group P63mc. Otherwise, with the addition of 1% Fe in the ZnO milled powder, the hexagonal ZnO phase remained unchanged, whereas the microstructural parameters were subject to significant variations due to the introduction of Fe atoms into the ZnO hexagonal matrix to replace oxygen ones. The size of crystallites and microstrains were milling time-dependent.
机译:ZnO粉末纳米颗粒掺有铁(通过机械合金化混合产生)。通过X射线衍射(XRD),扫描电子显微镜(SEM)和振动样品磁强法(VSM)研究了它们的结构,微观结构和磁性。起始原料为ZnO的纯粉末呈六方晶结构,空间群为P63mc。否则,在ZnO研磨粉中添加1%Fe时,六角形ZnO相保持不变,而由于将Fe原子引入ZnO六角形基体中代替氧原子,因此微观结构参数会发生重大变化。晶粒和微应变的大小取决于研磨时间。

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