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首页> 外文期刊>Electroanalysis >Square Wave Cathodic Adsorptive Stripping Voltammetric Determination of the Anticancer Drugs Flutamide and Irinotecan in Biological Fluids Using Renewable Pencil Graphite Electrodes
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Square Wave Cathodic Adsorptive Stripping Voltammetric Determination of the Anticancer Drugs Flutamide and Irinotecan in Biological Fluids Using Renewable Pencil Graphite Electrodes

机译：方波阴极吸附溶出伏安法使用可再生铅笔状石墨电极测定生物流体中的抗癌药氟他胺和伊立替康

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摘要

A sensitive electrochemical method based on square wave cathodic adsorptive stripping voltammetry (SWCASV) using pencil graphite electrodes (PGE) was developed for the individual and simultaneous determination of the anticancer drugs flutamide (Flu) and irinotecan (Irino) in biological fluids. Calibration curves showed an excellent linear response with limits of detection of 1.68 x 10(-9) and 1.55 x 10(-8) M Irino and Flu, respectively. The statistical evaluation of within-day repeatability (n=5) and day to day precision (n=5) showed satisfactory accuracy and precision. SWCASV using a PGE for individual and simultaneous determination of both drugs in bulk form, human urine and serum samples was demonstrated.
机译：建立了一种基于方波阴极吸附溶出伏安法（SWCASV）的灵敏电化学方法，该方法使用铅笔石墨电极（PGE）来单独测定生物流体中的抗癌药氟他胺（Flu）和伊立替康（Irino）。校准曲线显示了出色的线性响应，检测限分别为1.68 x 10（-9）和1.55 x 10（-8）M Irino和Flu。一天内重复性（n = 5）和日常精度（n = 5）的统计评估显示令人满意的精度和精度。证明了使用PGE的SWCASV可以同时单独测定散装形式，人尿和血清样品的两种药物。

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