Cocrystallization of C_(60) or C_(70) with the Bowl-Shaped Hydrocarbon Hexakis(E)?3,3-dimethyl-1-butenylbenzene To Form Chains of Clamshell Assemblies

Kamran B. Ghiassi; Susanne Y. Chen; Peter PrinzArmin de MeijereMarilyn M. OlmsteadAlan L. Balch

首页> 外文期刊>Crystal growth & design >Cocrystallization of C_(60) or C_(70) with the Bowl-Shaped Hydrocarbon Hexakis(E)?3,3-dimethyl-1-butenylbenzene To Form Chains of Clamshell Assemblies

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Cocrystallization of C_(60) or C_(70) with the Bowl-Shaped Hydrocarbon Hexakis(E)?3,3-dimethyl-1-butenylbenzene To Form Chains of Clamshell Assemblies

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The bowl-shaped hydrocarbon hexakis(E)-3,3-dimethyl-1-butenyl- benzene (HB) has been cocrystallized with either C_(60) or C_(70) to form clamshell-like assemblies with the fullerenes residing within the concave surfaces of two HB molecules. The structures of these two crystals have been determined by singlecrystal X-ray diffraction. The HB molecules exhibit back-to-back stacking and close contacts in both cocrystals. This trait is remarkably similar to the packing seen in cases in which fullerenes cocrystallize with M~(II)(OEP), where OEP is the dianion of octaethylporphyrin and M is generally Ni or Co. The C_(60) structure features an ordered cage with a disordered solvent position, while the C_(70) structure exhibits two orientations of the cage, all other components being ordered.

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《Crystal growth & design》 |2014年第8期|4005-4010|共6页
作者
Kamran B. Ghiassi; Susanne Y. Chen; Peter PrinzArmin de MeijereMarilyn M. OlmsteadAlan L. Balch;
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作者单位

Department of Chemistry, University of California, Davis, California 95616, United States;

Institut fu?r Organische und Biomolekulare Chemie, Georg-August-Universita?t Go?ttingen, Tammannstra?e 2, 37077 Go?ttingen, Germany;

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正文语种英语
中图分类晶体学;
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orientations; position; assemblies;

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Cocrystallization of C_(60) or C_(70) with the Bowl-Shaped Hydrocarbon Hexakis(E)?3,3-dimethyl-1-butenylbenzene To Form Chains of Clamshell Assemblies

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