Multistep synthesis of amides from alcohols and amines in continuous flow microreactor systems using oxygen and urea hydrogen peroxide as oxidants

Xiaoying Liu; Klavs F. Jensen

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Multistep synthesis of amides from alcohols and amines in continuous flow microreactor systems using oxygen and urea hydrogen peroxide as oxidants

机译：在氧气和尿素过氧化氢为氧化剂的连续流微反应器系统中，由醇和胺多步合成酰胺

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By integrating a heterogeneous oxidation step, gas-liquid separation, and an oxidative amidation reaction to form a continuous system, a multistep synthetic protocol has been demonstrated to produce amides under mild conditions using alcohols and amines as the starting materials. The use of inexpensive oxygen and urea hydrogen peroxide as the only oxidants affords an economical and adaptable synthetic route for amides.

机译：通过整合非均相氧化步骤，气液分离和氧化酰胺化反应以形成连续系统，已经证明了多步合成方案可在温和条件下使用醇和胺作为起始原料生产酰胺。使用廉价的氧气和过氧化氢脲作为唯一的氧化剂为酰胺提供了一种经济且适用的合成途径。

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《Green chemistry》 |2013年第6期|共4页
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Xiaoying Liu; Klavs F. Jensen;
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1. Multistep synthesis of amides from alcohols and amines in continuous flow microreactor systems using oxygen and urea hydrogen peroxide as oxidants [J] . Xiaoying Liu, Klavs F. Jensen Green chemistry . 2013,第6期

机译：在氧气和尿素过氧化氢为氧化剂的连续流微反应器系统中，由醇和胺多步合成酰胺
2. Direct oxidative amidation of aromatic aldehydes using aqueous hydrogen peroxide in continuous flow microreactor systems [J] . Xiaoying Liu, Klavs F. Jensen Green chemistry . 2012,第5期

机译：在连续流微反应器系统中，使用过氧化氢水溶液直接氧化芳香醛的酰胺化反应
3. Electrochemical multisensor system for monitoring hydrogen peroxide, hydrogen and oxygen in direct synthesis microreactors [J] . Sebastian Urban, Andreas Weltin, Hubert Flamm, Sensors and Actuators . 2018,第PTa927a184期

机译：电化学多传感器系统，用于监测直接合成微反应器中的过氧化氢，氢和氧
4. Kinetics of Hydrogen Peroxide Synthesis in a Microreactor by Direct Combination of Oxygen and Hydrogen [C] . Yury Voloshin, Adeniyi Lawal, Raghunath Halder Topical Conference on Applications of Micro-Reactor Engineering . 2007

机译：氧气和氢气直接组合微反应器中过氧化氢合成的动力学
5. Microchannel reactor system for synthesis of hydrogen peroxide by direct combination of hydrogen and oxygen [D] . Voloshin, Yury 2008

机译：通过氢和氧直接结合来合成过氧化氢的微通道反应器系统
6. Microwave-Accelerated Iodination of Some Aromatic Amines Using Urea-Hydrogen Peroxide Addition Compound (UHP) as the Oxidant [O] . Maciej Sosnowski, Lech Skulski 2002

机译：尿素-过氧化氢加成化合物（UHP）作为氧化剂对某些芳香胺进行微波加速的碘化
7. Multistep synthesis of amides from alcohols and amines in continuous flow microreactor systems using oxygen and urea hydrogen peroxide as oxidants [O] . Xiaoying Liu, Klavs F. Jensen 2013

机译：使用氧气和尿素过氧化氢作为氧化剂的连续流动微反应器系统中醇和胺的酰胺的多体合成

Multistep synthesis of amides from alcohols and amines in continuous flow microreactor systems using oxygen and urea hydrogen peroxide as oxidants

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