Highly efficient solvent-free acetylation of alcohols with acetic anhydride catalyzed by recyclable sulfonic acid catalyst (SBA-15-Ph-Pr-SO3H) - An environmentally benign method

Daryoush Zareyee; Abdollah Razaghi Ghadikolaee; Mohammad A. Khalilzadeh

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Highly efficient solvent-free acetylation of alcohols with acetic anhydride catalyzed by recyclable sulfonic acid catalyst (SBA-15-Ph-Pr-SO3H) - An environmentally benign method

机译：可循环利用的磺酸催化剂（SBA-15-Ph-Pr-SO3H）催化的乙酸酐对乙醇的高效无溶剂乙酰化-一种环保的方法

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摘要

The catalytic activity of highly thermal stable, hydrophobic, and complete heterogeneous propylsulfonic acid functionalized nanostructured SBA-15 for excellent acetylation of alcohols and phenols with acetic anhydride at ambient temperature in solvent-free conditions was examined under environmentally benign reaction conditions. The salient features of this protocol are the absence of solvent, a green experimental procedure, and simple reusability of the catalyst (at least five reaction cycles).

机译：在环境友好的反应条件下，在无溶剂的条件下，研究了高热稳定性，疏水性和完全多相丙基磺酸官能化的纳米结构SBA-15在醇和乙酸酐与乙酸酐的出色乙酰化作用下，在室温下的催化活性。该方案的显着特征是无溶剂，绿色实验程序和催化剂的简单可重复使用性（至少五个反应循环）。

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来源
《Canadian Journal of Chemistry》 |2012年第5期|共5页
作者
Daryoush Zareyee; Abdollah Razaghi Ghadikolaee; Mohammad A. Khalilzadeh;
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正文语种 eng
中图分类化学;
关键词
solid sulfonic acid; SBA-15; heterogeneous catalyst; acetylation; solvent-free.;

机译：固体磺酸;SBA-15;非均相催化剂;乙酰化;无溶剂;

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1. Highly efficient solvent-free acetylation of alcohols with acetic anhydride catalyzed by recyclable sulfonic acid catalyst (SBA-15-Ph-Pr-SO3H) - An environmentally benign method [J] . Daryoush Zareyee, Abdollah Razaghi Ghadikolaee, Mohammad A. Khalilzadeh Canadian Journal of Chemistry . 2012,第5期

机译：可循环利用的磺酸催化剂（SBA-15-Ph-Pr-SO3H）催化的乙酸酐对乙醇的高效无溶剂乙酰化-一种环保的方法
2. H6GeMo10V2O40?16H2O nanoparticles prepared by hydrothermal method: a new and reusable heteropoly acid catalyst for highly efficient acetylation of alcohols and phenols under solvent-free conditions [J] . Masoumeh Zaidi, Reza Zareisahamieh, Saeid Farhadi Journal of the Brazilian Chemical Society . 2011,第7期

机译：水热法制备的H6GeMo10V2O40？16H2O纳米颗粒：一种新型且可重复使用的杂多酸催化剂，用于在无溶剂条件下高效地乙酰化醇和酚
3. H6GeMo-(10)V_2O_(40)·16H_2O Nanoparticles Prepared by Hydrothermal Method: A New and Reusable Heteropoly Acid Catalyst for Highly Efficient Acetylation of Alcohols and Phenols under Solvent-Free Conditions [J] . Saeid Farhadi, Reza Zareisahamieh, Masoumeh Zaidi Journal of the Brazilian Chemical Society . 2011,第7期

机译：水热法制备的H6GeMo-（10）V_2O_（40）·16H_2O纳米颗粒：无溶剂条件下新型高效可重复使用的杂多酸催化剂，用于醇和苯酚的高效乙酰化
4. Highly efficient synthesis of symmetrical and unsymmetrical acyclic imides using 12-Tungstophosphorie acid as an environmentally benign and reusable catalyst [C] . Iraj Mohammadpoor-Baltork, Shahram Tangestaninejad, Majid Moghadam European Symposium on Organic Chemistry . 2009

机译：使用12-Tungstophorie酸作为环境良性和可重复使用的催化剂，高效合成对称和非对称无环酰亚胺
5. The use of new technologies to develop environmentally benign processes: Acid-catalyzed hydrolysis of pinene in aqueous media. [D] . Chamblee, Theresa S. 2004

机译：使用新技术开发对环境无害的方法：在水性介质中pin烯的酸催化水解。
6. Highly Efficient and Recyclable Catalysts for Cellobiose Hydrolysis: Systematic Comparison of Carbon Nanomaterials Functionalized With Benzyl Sulfonic Acids [O] . Samuel Carlier, Sophie Hermans 2020

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7. Acetylation of aromatic ethers using acetic anhydride over solid acid catalysts in a solvent-free system. Scope of the reaction for substituted ethers [O] . Smith Keith, El-Hiti Gamal A., Jayne Anthony J., 100

机译：在无溶剂体系中，使用乙酸酐在固体酸催化剂上乙酰化芳族醚。取代醚的反应范围

Highly efficient solvent-free acetylation of alcohols with acetic anhydride catalyzed by recyclable sulfonic acid catalyst (SBA-15-Ph-Pr-SO3H) - An environmentally benign method

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