首页> 外文期刊>Food and Bioproducts Processing. Transactions of the Institution of Chemical Engineers, Part C >Matching the nano- to the meso-scale: measuring deposit-surface interactions with atomic force microscopy and micromanipulation. (Special Issue: Fouling and cleaning in food processing 2010.)
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Matching the nano- to the meso-scale: measuring deposit-surface interactions with atomic force microscopy and micromanipulation. (Special Issue: Fouling and cleaning in food processing 2010.)

机译:使纳米级与中观级相匹配:利用原子力显微镜和显微操作测量沉积物-表面的相互作用。 (特刊:2010年食品加工中的结垢和清洁。)

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Many researchers have studied the effects of changing the surface on fouling and cleaning. In biofouling the 'Baier curve' is a well-known result which relates adhesion to surface energy, and papers on the effect of changing surface energy to food fouling can be found more than 40 years ago. Recently the use of modified surfaces, at least at a research level, has been widespread. Here two different ways of studying surface-deposit interactions have been compared. Atomic force microscopy (AFM) is a method for probing interactions at a molecular level, and can measure (for example) the interaction between substrate and surfaces at a nm-scale. At a micro m-mm level, we have developed a micromanipulation tool that can measure the force required to remove the deposit; the measure incorporates both surface and bulk deformation effects. The two methods have been compared by studying a range of model soils: toothpaste, as an example of a soil that can be removed by fluid flow alone, and confectionery soils. Removal has been studied from glass, stainless steel and fluorinated surfaces as examples of the sort of surfaces that can be found in practice. AFM measurements were made by using functionalized tips in force mode. The two types of probe give similar results, although the rheology of the soil affects the measurement from the micromanipulation probe under some circumstances. The data suggests that either method could be used to test candidate surfaces.
机译:许多研究人员研究了改变表面对结垢和清洁的影响。在生物污损中,“拜耳曲线”是一个众所周知的结果,它与表面能的附着力有关,而改变表面能对食物污损的影响的论文已有40多年的历史了。近年来,至少在研究水平上,已广泛使用改性表面。在这里,已经比较了研究表面沉积相互作用的两种不同方法。原子力显微镜(AFM)是一种在分子水平上探测相互作用的方法,可以以纳米级测量(例如)底物与表面之间的相互作用。我们已开发出微米级的微操作工具,可以测量去除沉积物所需的力;该措施兼顾了表面变形和整体变形的影响。通过研究各种模型污垢,对这两种方法进行了比较:牙膏(作为可以单独通过流体流动去除的污垢的示例)和糖果污垢。已经研究了从玻璃,不锈钢和氟化表面的去除方法,作为在实践中可以发现的表面类型的示例。使用力模式下的功能化尖端进行AFM测量。尽管土壤的流变学会在某些情况下影响微操作探针的测量,但两种类型的探针给出的结果相似。数据表明,这两种方法均可用于测试候选表面。

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