Determination of impurities in illicit methamphetamine samples seized in Iran

KhajeamiriA.R.; FaiziM.; SohaniF.; BaheriT.; KobarfardF.

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Determination of impurities in illicit methamphetamine samples seized in Iran

机译：伊朗缉获的非法甲基苯丙胺样品中杂质的测定

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In this study fifty samples of crystalline methamphetamine obtained from antinarcotics police of Iran seized during the year 2010 were analyzed. In order to determine the chemical characteristics of these samples, anion test, Gas Chromatography-Mass Spectrometry (GC-MS) and Liquid Chromatography-Mass Spectrometry (LC-MS) were carried out on the samples.All of the samples containing methamphetamine tested positive for chloride anion. The range of methamphetamine hydrochloride content in these samples was 33-95%. One sample out of 50 contained no methamphetamine.The fact that 1,2-dimethyl-3-phenylaziridine was the most frequently found impurity in the analyzed samples, indicates that most of the methamphetamine samples seized in Iran have been synthesized from pseudoephedrine as starting material.

机译：在这项研究中，分析了从伊朗禁毒警察局于2010年缉获的50种结晶甲基苯丙胺样品。为了确定这些样品的化学特性，对样品进行了阴离子测试，气相色谱-质谱（GC-MS）和液相色谱-质谱（LC-MS），所有含甲基苯丙胺的样品均呈阳性。氯离子。这些样品中盐酸甲基苯丙胺的含量范围为33-95％。 50个样本中没有一个含有甲基苯丙胺.1,2-二甲基-3-苯基氮丙啶是分析样品中最常见的杂质，这表明在伊朗缉获的大部分甲基苯丙胺样品均以伪麻黄碱为原料合成。

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来源
《Forensic science international》 |2012年第3期|共3页
作者
KhajeamiriA.R.; FaiziM.; SohaniF.; BaheriT.; KobarfardF.;
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正文语种 eng
中图分类 R89;
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Amphetamine-type stimulants (ATS); Gas chromatography-mass spectrometry (GC-MS); Liquid chromatography-mass spectrometry (LC-MS);

机译：苯丙胺类兴奋剂（ATS）;气相色谱-质谱（GC-MS）;液相色谱-质谱（LC-MS）;

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1. Determination of impurities in illicit methamphetamine samples seized in Iran [J] . KhajeamiriA.R., FaiziM., SohaniF., Forensic science international . 2012,第1a3期

机译：伊朗缉获的非法甲基苯丙胺样品中杂质的测定
2. SIMULTANEOUS HPLC DETERMINATION AND VALIDATION OF AMPHETAMINE, METHAMPHETAMINE, CAFFEINE, PARACETAMOL AND THEOPHYLLINE IN ILLICIT SEIZED TABLETS [J] . DR. MOHAMED SULTAN International Journal of Pharmacy and Pharmaceutical Sciences . 2014,第4期

机译：高效液相色谱法同时测定违禁片剂中安非他命，甲基苯丙胺，咖啡因，帕拉他莫尔和茶碱的含量
3. Impurity characteristics of street methamphetamine crystals seized in Tehran, Iran [J] . Shekari Ahmad, Akhgari Maryam, Jokar Farzaneh, Journal of substance use . 2016,第5期

机译：伊朗德黑兰缉获的甲基苯丙胺街头晶体的杂质特性
4. Automatic Screening of Major Impurities in Methamphetamine Samples Synthesized by Emde Method Using Accurate Mass Spectrometry [C] . Zhendong Hua, Wei Jia, Fengyun Pan, ASMS Conference on Mass Spectrometry and Allied Topics . 2014

机译：用精确质谱法自动筛选由EMDE方法合成的甲基苯丙胺样品中的主要杂质
5. Separation and identification of stereoisomers of methamphetamine and impurities of its illicit synthesis: 1,2-dimethyl-3-phenyl aziridine and chloroephedrine. [D] . Lekskulchai, Veeravan. 1999

机译：甲基苯丙胺及其非法合成杂质的立体异构体的分离和鉴定：1,2-二甲基-3-苯基氮丙啶和氯麻黄碱。
6. Identification of impurities and statistical classification of methamphetamine hydrochloride drugs seized in the China [O] . Jian Xin Zhang, Da Ming Zhang, Xu Guang Han -1

机译：在中国缉获的盐酸甲基苯丙胺药物的杂质鉴定和统计分类
7. Impurity Profiling of Street Methamphetamine Samples Seized in Kermanshah,Iran with Special Focus on Methamphetamine Impurities Health Hazards [O] . Neda Amini Afshar Etemadi 2015

机译：街道甲基苯丙胺样品的杂质谱分析，在Kermanshah，伊朗专注于甲基苯丙胺杂质健康危害
8. Analytical and Pharmacological Characterization of alpha-Benzyl-N-Methylphenethylamine, an Impurity in Illicit Methamphetamine Synthesis [R] . Moore, K. A. 1995

机译：α-苄基-N-甲基苯乙胺的分析和药理学表征，非法甲基苯丙胺合成中的杂质

Determination of impurities in illicit methamphetamine samples seized in Iran

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