Preconcentration of pentachlorophenol from sawdust using quinolin-8-ol immobilized on controlled-pore glass and determination by liquid chromatography

M.E.Leon-Gonzalez; L.V.Perez-Arribas; L.M.Polo-Diez; M.E.Silva-Vargas

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Preconcentration of pentachlorophenol from sawdust using quinolin-8-ol immobilized on controlled-pore glass and determination by liquid chromatography

机译：固定在控制孔玻璃上的喹啉-8-醇对木屑中的五氯苯酚进行预浓缩并通过液相色谱法测定

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A method for quantitative evaluation of penta- chlorophenol (PCP) in sawdust has been developed. Penta- chlorophenol is extracteQ from the solid matrix with 0.5 M sodium hydr{}xide and preconcentration was carried out using quinolin-8-o1 immobilized on controlled pore glass. Determi- nation was carried out by using liquid chFomatography with detection at 240 nm. Recoveries were between 84 and 97% at 1-3 #mu#g/g.

机译：已经开发了一种定量评估锯末中五氯苯酚（PCP）的方法。用0.5 M氢氧化钠从固体基质中萃取五氯苯酚，并使用固定在受控孔玻璃上的喹啉-8-o1进行预浓缩。使用液相色谱法在240 nm处进行检测。 1-3＃mu＃g / g的回收率在84％和97％之间。

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《Fresenius' Journal of Analytical Chemistry》 |2000年第1期|共3页
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M.E.Leon-Gonzalez; L.V.Perez-Arribas; L.M.Polo-Diez; M.E.Silva-Vargas;
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1. Preconcentration of pentachlorophenol from sawdust using quinolin-8-ol immobilized on controlled-pore glass and determination by liquid chromatography [J] . M.E.Leon-Gonzalez, L.V.Perez-Arribas, L.M.Polo-Diez, Fresenius' Journal of Analytical Chemistry . 2000,第1期

机译：固定在控制孔玻璃上的喹啉-8-醇对木屑中的五氯苯酚进行预浓缩并通过液相色谱法测定
2. Ionic liquid-based dispersive liquid-liquid microextraction combined with high performance liquid chromatography-UV detection for simultaneous preconcentration and determination of Ni, Co, Cu and Zn in water samples [J] . Asghari Alireza, Ghazaghi Mehri, Rajabi Maryam, Journal of the Serbian Chemical Society . 2014,第1期

机译：离子液体基分散液-液微萃取与高效液相色谱-紫外检测相结合，用于同时预富集和测定水中样品中的镍，钴，铜和锌
3. Determination of pentachlorophenol in certified waste waters, soil samples and industrial effluents using ELISA and liquid solid extraction followed by liquid chromatography [J] . Oubina A, Puig D, Gascon J, Analytica chimica acta . 1997,第1期

机译：使用ELISA和液相固体萃取-液相色谱法测定认证废水，土壤样品和工业废水中的五氯苯酚
4. Determination of diuretics in urine using immobilized-multiwalled carbon nanotubes hollow fiber liquid-phase microextraction combined with liquid chromatography-mass spectrometry [C] . Tse Tsung Ho, Maw Rong Lee American Society for Mass Spectrometry Conference on Mass Spectrometry and Allied Topics . 2012

机译：固定化 - 多壁碳纳米管中空纤维液相微萃取与液相色谱 - 质谱法测定尿液中的利尿剂测定
5. CHARACTERIZATION OF GLASS IMMOBILIZED 8-HYDROXYQUINOLINE FOR IN SITU PRECONCENTRATION OF TRACE METALS FROM AQUEOUS MEDIA. [D] . PAULSEN, KENNETH E. 1975

机译：玻璃固定化8-羟基喹啉的原位富集从介质中痕量金属的表征。
6. In-line system containing porous polymer monoliths for protein digestion with immobilized pepsin peptide preconcentration and nano-liquid chromatography separation coupled to electrospray ionization mass spectroscopy [O] . Laurent Geiser, Sebastiaan Eeltink, Frantisek Svec, -1

机译：包含多孔聚合物整体结构的在线系统用于固定化胃蛋白酶肽的预浓缩和纳米液相色谱分离与电喷雾电离质谱联用进行蛋白质消化
7. Ionic liquid-based dispersive liquid-liquid microextraction combined with high performance liquid chromatography-UV detection for simultaneous preconcentration and determination of Ni, Co, Cu and Zn in water samples [O] . Asghari Alireza, Ghazaghi Mehri, Rajabi Maryam, 2014

机译：离子液体分散液液微萃取结合高效液相色谱 - 紫外检测同时富集和测定水样中的镍，钴，铜和锌
8. Determination of Pentachlorophenol in Marine Biota and Sea Water by Gas-Liquid Chromatography and High-Pressure Liquid Chromatography [R] . Faas, L. F. , Moore, J. C. 1979

机译：气液色谱 - 高压液相色谱法测定海洋生物和海水中的五氯苯酚

Preconcentration of pentachlorophenol from sawdust using quinolin-8-ol immobilized on controlled-pore glass and determination by liquid chromatography

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