Transmission electron microscopy specimen preparation method for multiphase porous functional ceramics

Zhang W.; Kuhn L.T.; J?rgensen P.S.; Thydén K.; Bentzen J.J.; Abdellahi E.; Sudireddy B.R.; Chen M.; Bowen J.R.

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Transmission electron microscopy specimen preparation method for multiphase porous functional ceramics

机译：多相多孔功能陶瓷的透射电镜试样制备方法

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An optimum method is proposed to prepare thin foil transmission electron microscopy (TEM) lamellae of multiphase porous functional ceramics: prefilling the pore space of these materials with an epoxy resin prior to focused ion beam milling. Several advantages of epoxy impregnation are demonstrated by successful preparation of TEM specimens that maintain the structural integrity of the entire lamella. Feasibility of the TEM alignment procedure is demonstrated, and ideal TEM analyses are illustrated on solid oxide fuel cell and solid oxide electrolysis cell materials. Some potential drawbacks of the TEM specimen preparation method are listed for other samples.

机译：提出了一种制备多相多孔功能陶瓷薄箔透射电子显微镜（TEM）薄片的最佳方法：在聚焦离子束研磨之前用环氧树脂预填充这些材料的孔空间。通过成功地制备保持整个薄片结构完整性的TEM样品，证明了环氧浸渍的几个优点。证明了TEM对准程序的可行性，并说明了对固体氧化物燃料电池和固体氧化物电解电池材料的理想TEM分析。对于其他样品，列出了TEM样品制备方法的一些潜在缺点。

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《Microscopy and microanalysis: The official journal of Microscopy Society of America, Microbeam Analysis Society, Microscopical Society of Canada》 |2013年第2期|共5页
作者
Zhang W.; Kuhn L.T.; J?rgensen P.S.; Thydén K.; Bentzen J.J.; Abdellahi E.; Sudireddy B.R.; Chen M.; Bowen J.R.;
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正文语种 eng
中图分类分析化学;
关键词
epoxy; FIB; porous ceramic composites; TEM;

机译：环氧树脂;FIB;多孔陶瓷复合材料;TEM;

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1. Transmission electron microscopy specimen preparation method for multiphase porous functional ceramics [J] . Zhang W., Kuhn L.T., J?rgensen P.S., Microscopy and microanalysis: The official journal of Microscopy Society of America, Microbeam Analysis Society, Microscopical Society of Canada . 2013,第2期

机译：多相多孔功能陶瓷的透射电镜试样制备方法
2. A novel specimen preparation of porous cathode materials in lithium-ion batteries for high-resolution transmission electron microscopy [J] . Kim Na Yeon, Yim Taeeun, Lee Zonghoon Materials Characterization . 2019,第期

机译：高分辨率透射电子显微镜锂离子电池多孔阴极材料的新型样本制备
3. Specimen preparation of porous Au for transmission electron microscopy using cryo ion-milling. [J] . Tanabe T Journal of Electron Microscopy . 2011,第1期

机译：使用低温离子铣削的透射电子显微镜用多孔金的样品制备。
4. New methods of specimen preparation of pigment particles for investigations in transmission electron microscopy [C] . Lutz Berthold, Michael Krause, Martin Ebert, European technical coatings congress . 2014

机译：用于透射电子显微镜研究的颜料颗粒标本制备的新方法
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机译：陶瓷材料的透射和反射电子显微镜。
6. Biological Specimen Preparation for Transmission Electron Microscopy [O] . VISVAN NAVARATNAM 1999

机译：透射电子显微镜的生物标本制备
7. An Improved Specimen Preparation of Porous Powder Materials for Transmission Electron Microscopy [O] . Na Yeon Kim, Gyeong Hee Ryu, Hyo Ju Park, 2014

机译：一种改进的透射电子显微镜粉末材料制备
8. Polishing Methods for Metallic and Ceramic Transmission Electron Microscopy Specimens: Revision 1. [R] . Kestel, B. J. 1986

机译：金属和陶瓷透射电子显微镜样品的抛光方法：修订版1。

Transmission electron microscopy specimen preparation method for multiphase porous functional ceramics

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