High-Throughput Synthesis of Support Materials for Olefin Polymerization Catalyst

Chammingkwan Patchanee; Terano Minoru; Taniike Toshiaki

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High-Throughput Synthesis of Support Materials for Olefin Polymerization Catalyst

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摘要

Rational catalyst design necessitates fundamental knowledge on the structure-performance relationship, while the synthetic throughput for heterogeneous Ziegler-Natta olefin polymerization catalysts has long prevented the acquisition of a statistical database. In this contribution, an in-house reactor system was developed to realize the parallel synthesis of support materials for Ziegler-Natta catalysts for the first time. The developed system enabled parallel synthesis of 24 magnesium ethoxide samples with excellent reproducibility and morphological control comparable to a conventional experiment. Our demonstration revealed that the generation of diverse particle characteristics could be achieved through the addition of a third component as a structural modulator, in which the in-house parallel reactor system combined with the first principle component analysis enabled fast screening of effective modulators.

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来源
《ACS combinatorial science》 |2017年第5期|331-342|共12页
作者
Chammingkwan Patchanee; Terano Minoru; Taniike Toshiaki;
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作者单位

Japan Adv Inst Sci & Technol, Grad Sch Adv Sci & Technol, 1-1 Asahidai, Nomi, Ishikawa 9231292, Japan;

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原文格式 PDF
正文语种英语
中图分类化学;
关键词
high-throughput synthesis; spherical support; olefin polymerization; particle architecture; structural modulator;

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1. Extending the High-Throughput Experimentation (HTE) Approach to Catalytic Olefin Polymerizations: From Catalysts to Materials [J] . Vittoria Antonio, Urciuoli Gaia, Costanzo SalvatoreTammaro DanieleCannavacciuolo Felicia DanielaPasquino RossanaCipullo RobertaAuriemma FiniziaGrizzuti NinoMaffettone Pier LucaBusico Vincenzo Macromolecules . 2022,第12期

机译：Extending the High-Throughput Experimentation (HTE) Approach to Catalytic Olefin Polymerizations: From Catalysts to Materials
2. Synthesis of metallocene catalysts supported on polyp-(silylene)phenylene derivatives for the application to olefin polymerizations [J] . Hoang The Ban, Toshiya Uozumi, Tsuneji SanoKazuo Soga Macromolecular chemistry and physics . 1999,第8期

机译：Synthesis of metallocene catalysts supported on polyp-(silylene)phenylene derivatives for the application to olefin polymerizations
3. ChemInform Abstract: From Olefin Cyclopropanation to Olefin Metathesis Through Catalyst Engineering: Recent Applications of Olefin Metathesis to Fine Organic Synthesis and to Polymer Chemistry [J] . A. F. Noels, A. Demonceau Chem Inform . 1999,第13期

机译：ChemInform Abstract: From Olefin Cyclopropanation to Olefin Metathesis Through Catalyst Engineering: Recent Applications of Olefin Metathesis to Fine Organic Synthesis and to Polymer Chemistry
4. Synthesis of Optimal Technological Parameters of "Iron-Cast-Glass" Grinding Composite Materials Using Fuzzy Logic and Big Data Concepts [C] . T.G. Jabbarov, N.A. Gurbanov International Conference on Theory and Application of Fuzzy Systems and Soft Computing . 2021

机译：Synthesis of Optimal Technological Parameters of "Iron-Cast-Glass" Grinding Composite Materials Using Fuzzy Logic and Big Data Concepts
5. High-throughput screening of HZSM-5 supported metal-oxides catalysts for the coupling of methane with CO to benzene and naphthalene [O] . Wang H, Liu ZM, Shen JH, 2005

机译：High-throughput screening of HZsm-5 supported metal-oxides catalysts for the coupling of methane with CO to benzene and naphthalene

High-Throughput Synthesis of Support Materials for Olefin Polymerization Catalyst

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