Crystal structure of 3-2-(1,3-thia#173;zol-2-yl)diazen-1-ylpyridine-2,6-di#173;amine monohydrate

Chotima R.; Boonseng B.; Piyasaengthong A.Songsasen A.Chainok K.

首页> 外文期刊>Acta Crystallographica Section E: Crystallographic Communications >Crystal structure of 3-2-(1,3-thia#173;zol-2-yl)diazen-1-ylpyridine-2,6-di#173;amine monohydrate

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Crystal structure of 3-2-(1,3-thia#173;zol-2-yl)diazen-1-ylpyridine-2,6-di#173;amine monohydrate

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In the title hydrated azo compound, C8H8N6S#183;H2O, the two aromatic groups are close to coplanar with the dihedral angle between the mean planes of the thia#173;zole and pyridine rings being 2.9#8197;(2)#176;. The organic mol#173;ecule adopts an E configuration with respect to the double bond of the azo bridge. In the crystal, mol#173;ecules are linked by (amine)N#8212;H#8943;N(pyridine), (amine)N#8212;H#8943;O(water) and (water)O#8212;H#8943;N(thia#173;zole) hydrogen bonds along with #960;#8211;#960; inter#173;actions involving pairs of thia#173;zole rings and pairs of pyridine rings. The plane-to-plane distance between two parallel mol#173;ecules is 3.7856#8197;(4)#8197;#197; and corresponds to the length of the a axis. In this way, a layer structure parallel to (010) is formed. The layers are linked by weak C#8212;H#8943;S hydrogen bonds, eventually resulting in a three-dimensional network.

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《Acta Crystallographica Section E: Crystallographic Communications》 |2018年第4期|563-565|共3页
作者
Chotima R.; Boonseng B.; Piyasaengthong A.Songsasen A.Chainok K.;
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作者单位

Department of Chemistry, Faculty of Science, Naresuan University, Muang, Phitsanulok 65000, Thailand;

Department of Chemistry, Faculty of Science, Kasetsart University, Chatuchak, Bangkok 10900, Thailand;

Materials and Textile Technology, Faculty of Science and Technology, Thammasat University, Khlong Luang, Pathum Thani 12121, Thailand;

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正文语种英语
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CRYSTAL STRUCTURE; AZO DYES; HYDROGEN BONDING; PI-PI STACKING;

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Crystal structure of 3-2-(1,3-thia#173;zol-2-yl)diazen-1-ylpyridine-2,6-di#173;amine monohydrate

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