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Single-crystalline Ag_2V_4O_(11) nanobelts: hydrothermal synthesis, field emission, and magnetic properties

机译:Ag_2V_4O_(11)单晶纳米带:水热合成,场发射和磁性能

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摘要

A large number of single-crystalline Ag_2V_4O_(11) nanobelts with thickness of 10-30 nm, width of 70-200 nm, and lengths of 2-5 mu m have been successfully synthesized by a hydrothermal method. The morphologies and structures of the nanobelts were characterized by x-ray powder diffraction, x-ray photoelectron spectroscopy, transmission electron microscopy, high-resolution transmission electron microscopy, and thermal gravimetric analysis. The magnetic measurement data showed that Ag_2V_4O_(11) nanobelts are paramagnetic materials. The nanobelts exhibited an electronic emission turn-on field of 28.9 V mu m~(-1), which is the expected macroscopic field required to produce a current density of 10 mu A cm~(-2). On the basis of the analytical data, it was observed that Ag_2V_4O_(11) nanobelts could serve as a novel candidate for a future field emitter.
机译:通过水热法成功地合成了许多厚度为10-30 nm,宽度为70-200 nm,长度为2-5μm的单晶Ag_2V_4O_(11)纳米带。通过X射线粉末衍射,X射线光电子能谱,透射电子显微镜,高分辨率透射电子显微镜和热重分析对纳米带的形貌和结构进行了表征。磁测量数据表明,Ag_2V_4O_(11)纳米带是顺磁性材料。纳米带的电子发射导通场为28.9 Vμm·(-1),这是产生10μA cm·(-2)的电流密度所需的预期宏观场。根据分析数据,观察到Ag_2V_4O_(11)纳米带可以作为未来场发射器的新型候选物。

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