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Effects of focus change on the fabrication of tungsten nanowire by electron-beam-induced deposition

机译:焦点变化对电子束诱导沉积制备钨纳米线的影响

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摘要

The effects of focus change on the electron-beam-induced deposition (EBID) of tungsten nanowire in a scanning transmission electron microscope (STEM), were systematically investigated. By focusing the electron beam on the surface of carbon film, smooth tungsten nanowires were fabricated. The lateral size of the nanowire first decreased with the increase of beam scan speed, then became constant at about 7 nm when the scan speed was higher than 10 nm s~(-1). During the deposition of nanowire on carbon film, both overfocus and underfocus changes resulted in a conical profile with a central core line, whose deposition strongly depends on the electron dose. Broken wires can be fabricated by controlling the focus. For the deposition of self-supporting wire out of carbon film, the influence of focus change depended on the morphology of the deposited wire. Overfocus change can be used to keep the upward feature of the wire, while underfocus change is useful for the downward feature.
机译:在扫描透射电子显微镜(STEM)中系统地研究了焦点变化对钨纳米线电子束诱导沉积(EBID)的影响。通过将电子束聚焦在碳膜表面上,制成了光滑的钨纳米线。纳米线的横向尺寸首先随着束扫描速度的增加而减小,然后在扫描速度高于10 nm s〜(-1)时保持恒定在7 nm左右。在碳膜上沉积纳米线的过程中,过度聚焦和聚焦不足的变化都会导致圆锥形轮廓与中心核心线的接触,核心线的沉积很大程度上取决于电子剂量。可以通过控制焦点来制造断线。对于从碳膜中沉积自支撑金属丝,焦点变化的影响取决于所沉积金属丝的形态。过度聚焦变化可用于保持导线的向上特征,而过度聚焦变化可用于下降特征。

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