Probing the temperature dependence of the mechanical properties of polymers at the nanoscale with band excitation thermal scanning probe microscopy

Nikiforov MP; Jesse S; Morozovska AN; Eliseev EA; Germinario LT; Kalinin SV

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Probing the temperature dependence of the mechanical properties of polymers at the nanoscale with band excitation thermal scanning probe microscopy

机译：用带激发热扫描探针显微镜探测纳米级聚合物力学性能的温度依赖性

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Understanding local mechanisms for temperature-induced phase transitions in polymers requires quantitative measurements of the thermomechanical behavior, including glass transition and melting temperatures as well as temperature dependent elastic and loss modulus and thermal expansion coefficients in nanoscale volumes. Here, we demonstrate an approach for probing local thermal phase transitions based on the combination of thermal field confinement by a heated SPM probe and multi-frequency thermomechanical detection. The local measurement of the glass transition temperature is demonstrated and the detection limits are established.

机译：了解聚合物中温度引起的相变的局部机理需要对热机械行为进行定量测量，包括玻璃化转变和熔融温度以及与温度相关的弹性和损耗模量以及纳米级体积中的热膨胀系数。在这里，我们展示了一种基于加热SPM探针对热场限制和多频热机械检测相结合的探测局部热相变的方法。演示了玻璃化转变温度的本地测量并确定了检测极限。

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《Nanotechnology》 |2009年第39期|共10页
作者
Nikiforov MP; Jesse S; Morozovska AN; Eliseev EA; Germinario LT; Kalinin SV;
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正文语种 eng
中图分类特种结构材料;
关键词
SILICON MICROCANTILEVER HEATERS; ATOMIC-FORCE MICROSCOPE; NANOIMPRINT LITHOGRAPHY; EXPANSION MICROSCOPY; COMPOSITES; EVOLUTION; AFM;

机译：硅微悬臂加热炉;原子力显微镜;纳米压印术;膨胀显微镜;复合材料;演化;原子力显微镜;

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1. Probing the temperature dependence of the mechanical properties of polymers at the nanoscale with band excitation thermal scanning probe microscopy [J] . Nikiforov MP, Jesse S, Morozovska AN, Nanotechnology . 2009,第39期

机译：用带激发热扫描探针显微镜探测纳米级聚合物力学性能的温度依赖性
2. The band excitation method in scanning probe microscopy for rapid mapping of energy dissipation on the nanoscale [J] . Stephen Jesse, Sergei V Kalinin, Roger Proksch Nanotechnology . 2007,第43期

机译：扫描探针显微镜中的能带激发方法可在纳米尺度上快速绘制能量耗散图
3. The band excitation method in scanning probe microscopy for rapid mapping of energy dissipation on the nanoscale [J] . Jesse S, Kalinin SV, Proksch R, Nanotechnology . 2007,第43期

机译：扫描探针显微镜中的能带激发方法可在纳米尺度上快速绘制能量耗散图
4. Nanoscale Electronic Properties of a Model System and of a Conjugated Polymer Compound by Kelvin Probe Force Microscopy and Scanning Conductive Torsion Mode Microscopy [C] . Ling Sun, Jianjun Wang, Elmar Bonaccursor, American Chemical Society . 2010

机译：纳米级电子性质的模型系统和缀合的聚合物化合物通过开尔文探针力显微镜和扫描导电扭转模式显微镜
5. Probing the structure and nanoscale mechanical properties of polymer surfaces with Scanning Force Microscopy and Sum Frequency Vibrational Spectroscopy. [D] . Gracias, David Hugo. 1999

机译：用扫描力显微镜和和频振动光谱法探测聚合物表面的结构和纳米级机械性能。
6. Scanning probe acceleration microscopy (SPAM) in fluids: Mapping mechanical properties of surfaces at the nanoscale [O] . Justin Legleiter, Matthew Park, Brian Cusick, 2006

机译：流体中的扫描探针加速显微镜（SPAM）：绘制纳米级表面的机械性能
7. The band excitation method in scanning probe microscopy for rapid mapping of energy dissipation on the nanoscale [O] . Stephen Jesse, Sergei V Kalinin, Roger Proksch, 2007

机译：扫描探针显微镜的波段激发方法，用于快速映射纳米尺度
8. Probing the structure and nano-scale mechanical properties of polymer surfaces211 with scanning force microscopy and sum frequency vibrational spectroscopy [R] . Gracias, D. H. 1999

机译：用扫描力显微镜和和频振动光谱探讨聚合物表面211的结构和纳米尺度力学性能

Probing the temperature dependence of the mechanical properties of polymers at the nanoscale with band excitation thermal scanning probe microscopy

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