Pb(ZrxTi1-x)O-3 ceramics via reactive sintering of partially reacted mixture produced by a high-energy ball milling process

Kong LB.; Zhang TS.; Zhu W.Tan OK.Ma J.

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Pb(ZrxTi1-x)O-3 ceramics via reactive sintering of partially reacted mixture produced by a high-energy ball milling process

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Partially reacted mixtures of Pb(ZrxTi1-x)O-3 and its corresponding starting oxide components were obtained by a high-energy ball milling process. The partially reacted powders were characterized by x-ray diffraction and scanning electron microscopy techniques. The sintering behavior of the milled mixtures has demonstrated a distinct volumetric expansion before the densification of the samples, which clearly shows the occurrence of a reactive sintering process of the partially reacted powders. Such process requires a lower densification temperature as compared with the PZT powders produced by the conventional solid-state reaction process. PZT ceramics were found to form directly from the partially reacted powders sintered at 900-1200 degreesC. The dielectric and ferroelectric properties of the PZT ceramics as a function of sintering temperature and milling time were also studied and discussed. References: 26

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《Journal of Materials Research》 |2001年第6期|1636-1643|共8页
作者
Kong LB.; Zhang TS.; Zhu W.Tan OK.Ma J.;
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作者单位

Nanyang Technol Univ, Sch Mat Engn, Singapore 639798, Singapore, .;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
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正文语种英语
中图分类工程材料学;
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Pb(ZrxTi1-x)O-3 ceramics via reactive sintering of partially reacted mixture produced by a high-energy ball milling process

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