Catalytic transfer hydrogenation of aromatic nitro compounds in presence of polymer-supported nano-amorphous Ni-B catalyst

Hongliang Wen; Kaisheng Yao; Yingdan Zhang

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Catalytic transfer hydrogenation of aromatic nitro compounds in presence of polymer-supported nano-amorphous Ni-B catalyst

机译：聚合物负载的纳米非晶态Ni-B催化剂存在下芳香硝基化合物的催化转移加氢

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摘要

Polymer-supported nano-amorphous Ni-B particles prepared by ion-exchange-chemical reduction method exhibited good activity in the catalytic transfer hydrogenation of aromatic nitro compounds with hydrazine hydrate as hydrogen donor. The catalyst was characterized by ICP, SEM, TEM, XRD and XPS. The reusability experiments showed that the catalyst was stable and could be used three times with no decrease in activity.

机译：通过离子交换化学还原法制备的聚合物负载的纳米非晶态Ni-B颗粒在以水合肼为氢供体的芳香族硝基化合物的催化转移加氢中表现出良好的活性。通过ICP，SEM，TEM，XRD和XPS对催化剂进行了表征。可重复使用性实验表明，该催化剂稳定，可以使用3次而活性没有降低。

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《Catalysis Communications》 |2009年第8期|共5页
作者
Hongliang Wen; Kaisheng Yao; Yingdan Zhang;
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正文语种 eng
中图分类化学工业;
关键词
Catalytic transfer hydrogenation; Aromatic nitro compounds; Anilines; Polymer-supported; Nano-amorphous Ni-B;

机译：催化转移加氢芳香硝基化合物苯胺聚合物负载纳米非晶态Ni-B;

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专利

1. Catalytic transfer hydrogenation of aromatic nitro compounds in presence of polymer-supported nano-amorphous Ni-B catalyst [J] . Hongliang Wen, Kaisheng Yao, Yingdan Zhang Catalysis Communications . 2009,第8期

机译：聚合物负载的纳米非晶态Ni-B催化剂存在下芳香硝基化合物的催化转移加氢
2. Polymer-supported formate and zinc: A novel system for the transfer hydrogenation of aromatic nitro compounds [J] . G R Srinivasa, K Abiraj, D Channe Gowda Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2006,第1期

机译：聚合物支撑的甲酸和锌：转移芳香族硝基化合物的新型系统
3. Transfer Hydrogenation of Aromatic Nitro Compounds Using Polymer-Supported Formate and Pd-C [J] . K.Abiraj, G.R.Srinivasa, D.Channe Gowda Synthetic Communications . 2005,第2期

机译：高分子支持的甲酸酯和Pd-C转移芳族硝基化合物
4. LIQUID-PHASE CATALYTIC TRANSFER HYDROGENATION OF AROMATIC NITRO COMPOUNDS OVER NICKEL-DOPED CARBON CATALYSTS [C] . Li Xing, Jieshan Qiu, Yangying Chen, International Carbon Conference(Carbon 2007); 20070715-20; Seattle,WA(US) . 2007

机译：镍掺杂碳催化剂上芳族硝基化合物的液相催化转移加氢
5. CARBOHYDRAZIDE AS A SOLID REDUCING AGENT FOR REACTION GAS CHROMATOGRAPHY (DETERMINATION OF AZO, NITRO AND SULFONATE COMPOUNDS). PART I: REACTIONGAS CHROMATOGRAPHY OF AZO COMPOUNDS BY CARBOHYDRAZIDE REDUCTION AND GAS CHROMATOGRAPHY OF THE RESULTANT COMPOUNDS. PART II: ANALYSIS OF AROMATIC NITRO COMPOUNDS AND AROMATIC SULFONATES BY CARBOHYDRAZIDE REDUCTION AND GAS CHROMATOGRAPHY OF THE RESULTANT COMPOUNDS. [D] . RAHN, PETER CHARLES. 1973

机译：碳酰肼作为一种固体还原剂，用于气相色谱法（测定偶氮，硝基和磺酸盐化合物）。第一部分：偶氮化合物通过碳酰肼还原反应的气相色谱法和所得化合物的气相色谱法。第二部分：用碳酰肼还原法和气相色谱法分析芳香族硝基化合物和芳香族硫酸酯。
6. Preparation of sub-microspherical Fe3O4@PDA-Pd NPs catalyst and application in catalytic hydroreduction reaction of halogenated aromatic nitro compounds to prepare halogenated aromatic amines [O] . Haichang Guo, Renhua Zheng, Huajiang Jiang, 2019

机译：亚微球Fe3O4 @ PDA-Pd NPs催化剂的制备及其在卤代硝基硝基化合物催化加氢还原反应中的应用
7. Polymer-Supported Formate and Zinc: A Novel System for the Transfer Hydrogenation of Aromatic Nitro Compounds. [O] . G. R. Srinivasa, K. Abiraj, D. Channe Gowda 2006

机译：聚合物负载的甲酸盐和锌：一种用于转移氢化芳族硝基化合物的新型系统。
8. Selective Catalytic Hydrogenation of Polynuclear Heteroaromatic Compounds Using Polymer-Supported Transition-Metal Compounds as Catalyst. [R] . Fish, R. H., Heinemann, H. 1985

机译：用聚合物负载的过渡金属化合物作催化剂选择性催化加氢多核杂芳族化合物。

Catalytic transfer hydrogenation of aromatic nitro compounds in presence of polymer-supported nano-amorphous Ni-B catalyst

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