2,6-Bis(S)-4-benzyl-4,5-dihydro-1,3-oxazol-2-ylpyridine

Beller M.; Junge K.; M#246ller K.Spannenberg A.

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2,6-Bis(S)-4-benzyl-4,5-dihydro-1,3-oxazol-2-ylpyridine

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The commercially available title compound, C25H23N3O2, has been known since 1993 Nesper et al. (1993). Helv. Chim. Acta, 76, 2239–2249, but has not been structurally characterized until now. In the free ligand, the N atoms of both oxazoline rings point in opposite directions. The phenyl rings make dihedral angles of 30.56 (5) and 84.57 (3)° with the pyridine ring and 72.85 (3)° with each other.

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《Acta Crystallographica Section E: Crystallographic Communications》 |2011年第5期|o1181-o1181|共页
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Beller M.; Junge K.; M#246ller K.Spannenberg A.;
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1. ChemInform Abstract: Stereoselectivity in Reactions of Metal Complexes. Part 17. Synthesis of Three New Optically Active Triamines: 2,6‐Bis(((2S)‐2‐( hydroxymethyl)pyrrolidin‐1‐yl)methyl)pyridine, 2,6‐Bis(((2S)‐2‐( methoxymethyl)pyrrolidin‐1‐yl)methyl)pyridine, and 2,6‐Bis(((2S)‐2‐(( benzyloxy)methyl)pyrrolidin‐1‐yl)methyl)pyridine. X‐Ray Structure and Equilibrium Behavior of Their Copper(II) Complexes. [J] . K. BERNAUER, T. CHUARD, H. STOECKLI‐EVANS Chem Inform . 1993,第52期

机译：ChemInform Abstract: Stereoselectivity in Reactions of Metal Complexes. Part 17. Synthesis of Three New Optically Active Triamines: 2,6‐Bis(((2S)‐2‐( hydroxymethyl)pyrrolidin‐1‐yl)methyl)pyridine, 2,6‐Bis(((2S)‐2‐( methoxymethyl)pyrrolidin‐1‐yl)methyl)pyridine, and 2,6‐Bis(((2S)‐2‐(( benzyloxy)methyl)pyrrolidin‐1‐yl)methyl)pyridine. X‐Ray Structure and Equilibrium Behavior of Their Copper(II) Complexes.
2. Stereoselectivity in Reactions of Metal Complexes. Part XVII. Synthesis of three new optically active triamines: 2,6‐Bis{(2S)‐2‐(hydroxymethyl)pyrrolidin‐1‐ylmethyl}pyridine, 2,6‐bis{(2S)‐2‐(methoxymethyl)pyrrolidin‐1‐ylmethyl}pyridine, and 2,6‐bis{{(2S)‐2‐(benzyloxy)methylpyrrolidin‐1‐yl}methyl}pyridine. X‐ray structure and equilibrium behaviour of their copper(II) complexes [J] . Klaus Bernauer, Thierry Chuard, Helen Stoeckli‐Evans helvetica chimica acta . 1993,第6期

机译：Stereoselectivity in Reactions of Metal Complexes. Part XVII. Synthesis of three new optically active triamines: 2,6‐Bis{(2S)‐2‐(hydroxymethyl)pyrrolidin‐1‐ylmethyl}pyridine, 2,6‐bis{(2S)‐2‐(methoxymethyl)pyrrolidin‐1‐ylmethyl}pyridine, and 2,6‐bis{{(2S)‐2‐(benzyloxy)methylpyrrolidin‐1‐yl}methyl}pyridine. X‐ray structure and equilibrium behaviour of their copper(II) complexes
3. Synthesis and lanthanide coordination properties of new 2,6-bis(N-tert-butylacetamide)pyridine and 2,6-bis(N-tert-butylacetamide)pyridine-N-oxide ligands [J] . Binyamin I, Pailloux S, Duesler ENRapko BMPaine RT Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 2006,第15期

机译：Synthesis and lanthanide coordination properties of new 2,6-bis(N-tert-butylacetamide)pyridine and 2,6-bis(N-tert-butylacetamide)pyridine-N-oxide ligands
4. Search for a One-Electron Reduction of the Cation Radical of an "Extended Viologen",p-Phenylene-bis-4,4'-(1-Aryl-2,6-Diphenylpyridinium) [C] . L. Pospisil, J. Fiedler, M. Hromadova, Meeting of the Electrochemical Society . 2007

机译：搜索“延长viologen”，对亚苯基-BIS-4,4' - （1-芳基-2,6-二苯基吡啶鎓）的阳离子的单电子减少
5. Tridentate nitrogen ligands derived from 2,6-bis-hydrazinopyridine (BHP): Preparation and study of the 2,6-bis-hydrazonopyridines, 2,6-bis-pyrazolylpyridines, and 2,6-bis-indazolylpyridines. [D] . Duncan, Nathan C. 2009

机译：源自2,6-双-肼基吡啶（BHP）的三齿氮配体：2,6-双-肼基吡啶，2,6-双-吡唑基吡啶和2,6-双-吲唑基吡啶的制备和研究。
6. 4-(4-Bromophenyl)-2,6-diphenylpyridine [O] . Qun Cao, Yu Xie, Jie Jia, 2016

机译：4-(4-Bromophenyl)-2,6-diphenylpyridine
7. catena-Poly[[bis(nitrato-κO)copper(II)]-μ-1,4-bis(4,5-dihydro-1,3-oxazol-2-yl)benzene-κ2N:N′] [O] . Pin-Ning Wang, Chun-Wei Yeh, Hui-An Tsai, 2011

机译：catena-Poly [[bis（nitrato-＆＃954; O）copper（II）]-＆＃956; -1,4-bis（4,5-dihydro-1,3-oxazol-2-yl）benzene- ＆＃954; 2N：N＆＃8242;]
8. Syntheses of Pentacyclo(5.4.0.0(2,6).0(3,10).O(5,9))undecane-4,8,11-trione, Pentacyclo(6.3.0.0(2,6).0(3,10).0(5,9))undecane-4,7,11-trione (D3-Trishomocubanetrione), and 4,4,7,7,11,11-Hexanitro(6.3.0.0(2,6).0(3,10).0(5,9)undecane ( [R] . Marchand, A. P., Sharma, G. V., Annapurna, G. S., 1987

机译：合成五环（5.4.0.0（2,6）.0（3,10）.O（5,9））十一烷-4,8,11-三酮，五环（6.3.0.0（2,6）.0（ 3,10）.0（5,9））十一烷-4,7,11-三酮（D3-Trishomocubanetrione）和4,4,7,7,11,11-Hexanitro（6.3.0.0（2,6）） .0（3,10）.0（5,9）undecane（

2,6-Bis(S)-4-benzyl-4,5-dihydro-1,3-oxazol-2-ylpyridine

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