Grafting of a tetrahydro-salen copper(II)complex on surface modified mesoporous materials and its catalytic behaviour

Ayyamperumal Sakthivel; Wei Sun; Gabriele Raudaschl-Sieber; Anthony S.T.Chiang; Marianne Hanzlik

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Grafting of a tetrahydro-salen copper(II)complex on surface modified mesoporous materials and its catalytic behaviour

机译：表面改性介孔材料上的四氢salen铜（II）配合物的接枝及其催化行为

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A tetrahydro-salen copper(n)complex(1)is grafted on the iodosilane modified surfaces of MCM-41 and MCM-48.The presence of complex 1 on the surfaces is evidenced by ~1H MAS-NMR,elemental analysis and TG-MS.The strucutre of the supports after modification remains intact,which is evident from powder XRD,N_2 adsorption/desorption(BET),and TEM analysis.The grafted materials are applicable as catalysts for cyclooctene epoxidation and they are found to maintain activity for several runs.

机译：在MCM-41和MCM-48的碘硅烷改性表面上接枝了四氢沙仑铜（n）络合物（1）。〜1H MAS-NMR，元素分析和TG- MS。改性后的载体结构保持完好无损，这从粉末XRD，N_2吸附/解吸（BET）和TEM分析可以明显看出。接枝的材料可用作环辛烯环氧化的催化剂，发现它们可以保持多种活性运行。

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来源
《Catalysis Communications》 |2006年第5期|共6页
作者
Ayyamperumal Sakthivel; Wei Sun; Gabriele Raudaschl-Sieber; Anthony S.T.Chiang; Marianne Hanzlik;
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正文语种 eng
中图分类化学工业;
关键词
Tetrahydro-salen Cu(II)complex; Olefin epoxidation; Mesoporous materials; Grafting;

机译：四氢salen Cu（II）络合物;烯烃环氧化;介孔材料;接枝;

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1. Grafting of a tetrahydro-salen copper(II)complex on surface modified mesoporous materials and its catalytic behaviour [J] . Ayyamperumal Sakthivel, Wei Sun, Gabriele Raudaschl-Sieber, Catalysis Communications . 2006,第5期

机译：表面改性介孔材料上的四氢salen铜（II）配合物的接枝及其催化行为
2. New hybrid materials based on the grafting of Pd(II)-amino complexes on the graphitic surface of AC: preparation, structures and catalytic properties [J] . Luz Godino-Salido M., Gutierrez-Valero Maria D., Lopez-Garzon Rafael, RSC Advances . 2016,第63期

机译：基于Pd（II）-氨基络合物在AC的石墨表面接枝的新型混合材料：制备，结构和催化性能
3. New hybrid materials based on the grafting of Pd(ii)-amino complexes on the graphitic surface of AC: preparation, structures and catalytic properties [J] . M. Luz Godino-Salido, María D. Gutiérrez-Valero, Rafael López-Garzón, RSC Advances . 2016,第63期

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6. Isolation and immobilization of alkaline protease on mesoporous silica and mesoporous ZSM-5 zeolite materials for improved catalytic properties [O] . Arpana Kumari, Balwinder Kaur, Rajendra Srivastava, 2015

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7. New hybrid materials based on the grafting of Pd(II)-amino complexes on the graphitic surface of AC: preparation, structures and catalytic properties [O] . Godino-Salido, M. Luz, Gutiérrez-Valero, María D., López-Garzón, Rafael, 2016

机译：基于AC石墨表面接枝Pd（II）-氨基配合物的新型杂化材料：制备，结构和催化性能

Grafting of a tetrahydro-salen copper(II)complex on surface modified mesoporous materials and its catalytic behaviour

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