Montmorillonite KSF clay as an efficient catalyst for the synthesis of 1,4-dioxo-3,4-dihydrophthalazine-2(1H)-carboxamides and -carbothioamides under solvent-free conditions using microwave irradiation

Davood Habibi; Omid Marvi

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Montmorillonite KSF clay as an efficient catalyst for the synthesis of 1,4-dioxo-3,4-dihydrophthalazine-2(1H)-carboxamides and -carbothioamides under solvent-free conditions using microwave irradiation

机译：蒙脱土KSF粘土是在无溶剂条件下使用微波辐射合成1,4-二氧代-3,4-二氢邻苯二甲酸2（1H）-羧酰胺和-碳硫代酰胺的有效催化剂

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摘要

Different 1,4-dioxo-3,4-dihydrophthalazine-2(1H)-carboxamide and-carbothioamide derivatives were synthesized in a simple and environmentally benign method from the reaction of different phthalic anhydrides with semicarbazide or thiosemicarbazide using montmorillonite KSF clay as solid acidic catalyst and microwave irradiations under the solvent-free conditions in good yields and short reaction times.

机译：以蒙脱土KSF粘土为固体酸性，通过不同邻苯二甲酸酐与氨基脲或硫代氨基脲的反应，以一种简单且环境友好的方法合成了不同的1,4-二氧代-3,4-二氢邻苯二甲酸-2（1H）-羧酰胺和碳硫代酰胺衍生物。在无溶剂条件下以高产率和短反应时间进行催化剂和微波辐射。

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来源
《Catalysis Communications》 |2007年第26期|共4页
作者
Davood Habibi; Omid Marvi;
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正文语种 eng
中图分类化学工业;
关键词
Montmorillonite KSF clay; Phthalic anhydrides; Semicarbazide; Thiosemicarbazide;

机译：蒙脱石KSF粘土;邻苯二甲酸酐;氨基脲;硫代氨基脲;

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1. Montmorillonite KSF clay as an efficient catalyst for the synthesis of 1,4-dioxo-3,4-dihydrophthalazine-2(1H)-carboxamides and -carbothioamides under solvent-free conditions using microwave irradiation [J] . Davood Habibi, Omid Marvi Catalysis Communications . 2007,第26期

机译：蒙脱土KSF粘土是在无溶剂条件下使用微波辐射合成1,4-二氧代-3,4-二氢邻苯二甲酸2（1H）-羧酰胺和-碳硫代酰胺的有效催化剂
2. Microwave-Induced Solvent-free Synthesis of -Keto Esters Using Montmorillonite KSF and K10 Clays as Efficient and Recyclable Heterogeneous Solid Acids [J] . Omid MARVI, Davood HABIBI Chinese Journal of Chemistry . 2008,第3期

机译：用蒙脱土KSF和K10粘土作为高效可回收的非均相固体酸的微波诱导无溶剂合成酮基酯
3. Microwave-Induced Solvent-free Synthesis of β-Keto Esters Using Montmorillonite KSF and K10 Clays as Efficient and Recyclable Heterogeneous Solid Acids [J] . MARVI Omid, HABIBI Davood 中国化学（英文版） . 2008,第003期

机译：蒙脱土KSF和K10粘土作为高效可回收的非均相固体酸的微波诱导无溶剂合成β-酮酯
4. Coaled carbon-based solid acid: A new and efficient catalyst for click synthesis of 3,4-dihydropyrimidin-2(1H)-ones under solvent-free conditions [C] . Liu Wanyi, Ning Liu, Ruiyuan Zheng, International Conference on Chemical, Material and Metallurgical Engineering . 2013

机译：含有碳化碳固体酸：在无溶剂条件下单击合成3,4-二氢嘧啶-2（1H）酮的新增有效的催化剂
5. New developments toward the synthesis of heterocycles and applications in green chemistry. I. A simple and essentially one-pot synthesis of N-aminated heterocycles using phase transfer catalyst (Aliquat-336). II. Synthesis of pharmaceutically important pyrrole derivatives. III. Applications in green chemistry: Surfactant-mediated environmentally friendly cleavage of aromatic esters and trans-esterification under solvent-free neutral conditions . [D] . Patel, Nitinchandra. 2005

机译：杂环合成的新进展及其在绿色化学中的应用。 I.使用相转移催化剂（Aliquat-336）简单且基本上一锅合成N-胺化的杂环。二。药学上重要的吡咯衍生物的合成。三，在绿色化学中的应用：在无溶剂的中性条件下，表面活性剂介导的环境友好的芳族酯裂解和酯交换反应。
6. Recyclable Keggin Heteropolyacids as an Environmentally Benign Catalyst for the Synthesis of New 2-Benzoylamino-N-phenyl-benzamide Derivatives under Microwave Irradiations at Solvent-Free Conditions and the Evaluation of Biological Activity [O] . Karima Ighilahriz-Boubchir, Baya Boutemeur-Kheddis, Cherifa Rabia, 2018

机译：无溶剂条件下可回收的Keggin杂多酸作为环境友好的催化剂用于在无溶剂条件下微波辐射下合成新的2-苯甲酰基氨基-N-苯基-苯甲酰胺衍生物。
7. Montmorillonite KSF and montmorillonite K-10 clays as efficient catalysts for the solventless synthesis of bismaleimides and bisphthalimides using microwave irradiation [O] . Davood Habibi, Omid Marvi 2006

机译：蒙脱石KsF和蒙脱土K-10粘土作为微波辐射无溶剂合成双马来酰亚胺和双酞亚胺的有效催化剂

Montmorillonite KSF clay as an efficient catalyst for the synthesis of 1,4-dioxo-3,4-dihydrophthalazine-2(1H)-carboxamides and -carbothioamides under solvent-free conditions using microwave irradiation

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