Endurance Tests and Kinetic Experiment in a Plug-Flow Reactor with a Fixed Catalyst Bed

E. A. Karalin; A. V. Oparkin; A. G. Abramov; S. B. Pavlov; N. F. Murtazin; D. M. Appakova; D. V. Ksenofontov; N. P. Miroshkin; Kh. E. Kharlampidi

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Endurance Tests and Kinetic Experiment in a Plug-Flow Reactor with a Fixed Catalyst Bed

机译：具有固定催化剂床的塞流反应器的耐久性试验和动力学实验

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As an example of the liquid-phase hydrogenation of methyl-phenol ketone to 1-phenylethanol, variants of the construction of a pilot reactor are considered for performing long-term tests of heterogeneous catalysts of a fixed bed. Calculations for the reactor unit during hydrogenation on NTK-11 are presented as an example. It is shown that a cascade of three adiabatic reactors with a catalyst bed height of 4.5 m each is needed to ensure a residual reactant concentration below 1 wt %.

机译：作为甲基苯酚酮液相加氢成1-苯基乙醇的一个例子，考虑了中试反应器构造的变体，以进行固定床非均相催化剂的长期测试。以NTK-11氢化过程中反应器单元的计算为例。结果表明，需要三个级联的绝热反应器，每个催化剂床的高度为4.5 m，以确保残留的反应物浓度低于1 wt％。

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来源
《Catalysis in industry》 |2016年第3期|共6页
作者
E. A. Karalin; A. V. Oparkin; A. G. Abramov; S. B. Pavlov; N. F. Murtazin; D. M. Appakova; D. V. Ksenofontov; N. P. Miroshkin; Kh. E. Kharlampidi;
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正文语种 eng
中图分类物理化学（理论化学）、化学物理学;
关键词
methyl-phenol ketone; hydrogenation; heterogeneous catalysis; fixed-bed reactor; mathematical model;

机译：甲基苯酚酮加氢非均相催化固定床反应器数学模型;

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1. Endurance Tests and Kinetic Experiment in a Plug-Flow Reactor with a Fixed Catalyst Bed [J] . E. A. Karalin, A. V. Oparkin, A. G. Abramov, Catalysis in industry . 2016,第3期

机译：具有固定催化剂床的塞流反应器的耐久性试验和动力学实验
2. Simultaneous Measurement of X-ray Absorption Spectra and Kinetics: A Fixed-bed, Plug-flow Operando Reactor [J] . Bradley R. Fingland, Fabio H. Ribeiro, Jeffrey T. Miller Catalysis Letters . 2009,第1a2期

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3. Liquid phase propylene epoxidation with H2O2 on TS-1/SiO2 catalyst in a fixed-bed reactor: experiments and deactivation kinetics [J] . Feng Wenping, Wang Yaquan, Wu Guoqiang, Journal of Chemical Technology & Biotechnology . 2015,第8期

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5. THE MODELING AND DYNAMICS OF CATALYSTS AND FIXED BED REACTORS. [D] . JENSEN, KLAVS FLEMMING. 1980

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机译：钴F-T催化剂的技术开发。专题报告3，氧化锆促进费 - 托钴催化剂：在固定床和浆料鼓泡塔反应器中的行为

Endurance Tests and Kinetic Experiment in a Plug-Flow Reactor with a Fixed Catalyst Bed

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