Norfloxacin-derivative functionalized octamolybdate: unusual carbonyl coordination and acidity sensitive luminescence

Liu Hong; Chai Dong-Feng; Zou Yu-Long; Zhou Shu-Jing; Wang Wei; Shen De-Feng; Qu Yan-Yan; Gao Guang-Gang

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Norfloxacin-derivative functionalized octamolybdate: unusual carbonyl coordination and acidity sensitive luminescence

机译：诺氟沙星衍生物官能化的钼酸钼：异常的羰基配位和对酸度敏感的发光

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A novel gamma-type octamolybdate functionalized by decarboxylated norfloxacin (dNF), (dNF)(2)[gamma-Mo8O26(dNF)(2)]center dot 10H(2)O (1), has been synthesized. In the broad range of acidic solutions, even in the pH < 0 range, the fluorescent intensities of 1 almost linearly changed with acidity, indicating that a solution of 1 could be used as an acidity fluorescent sensor. The enhancing and quenching behavior also makes complex 1 a potential acid-base switch system. The successful synthesis of 1 demonstrates a new acidity sensor based on a fluorescent medicine and polyoxometalate anions.

机译：合成了由脱羧诺氟沙星（dNF），（dNF）（2）[γ-Mo8O26（dNF）（2）]中心点10H（2）O（1）功能化的新型γ型八钼酸盐。在宽范围的酸性溶液中，即使在pH <0范围内，荧光强度1几乎随酸度线性变化，这表明溶液1可以用作酸性荧光传感器。增强和淬灭行为也使复合物1成为潜在的酸碱转换系统。 1的成功合成证明了一种基于荧光药物和多金属氧酸盐阴离子的新型酸度传感器。

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《RSC Advances》 |2015年第51期|共4页
作者
Liu Hong; Chai Dong-Feng; Zou Yu-Long; Zhou Shu-Jing; Wang Wei; Shen De-Feng; Qu Yan-Yan; Gao Guang-Gang;
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1. Norfloxacin-derivative functionalized octamolybdate: unusual carbonyl coordination and acidity sensitive luminescence [J] . Liu Hong, Chai Dong-Feng, Zou Yu-Long, RSC Advances . 2015,第51期

机译：诺氟沙星衍生物官能化的钼酸钼：异常的羰基配位和对酸度敏感的发光
2. Carbonyl coordination chemistry from a new angle: A computational study of alpha-carbon acidity based on electrophile coordination geometry [J] . Houk RJT, Anslyn EV, Stanton JF Organic letters . 2006,第16期

机译：羰基配位化学的新视角：基于亲电子配位几何结构的α-碳酸度计算研究
3. Holmium, thulium and lutetium-octamolybdate [Mo8O28](8-) 1D chains: luminescence investigation of europium doped lutetium-octamolybdate [J] . Kaczmarek Anna M., Van Deun Rik, Van Hecke Kristof Dalton transactions: An international journal of inorganic chemistry . 2019,第23期

机译：Holmium，Thulium和Lutetium-Octamolybdate [Mo8O28]（8-）1D链：发光调查铕的Lutetium-Octamolybdate
4. New. Selective Transformation Reactions of Imino and Carbonyl Functionalities Using Coordination Abilities of Metals [C] . Makoto SHIMIZU 10th international symposium on fine chemistry and functional polymers . 2000

机译：新。利用金属的配位能力进行氨基和羰基官能团的选择性转化反应
5. Manganese carbonyl hydrosilation catalysis: Reducing organic carbonyl functionalities. [D] . Punia, Surinder S. 2004

机译：羰基锰硅氢化反应：降低有机羰基官能度。
6. Carbonyl-twisted 6-acyl-2-dialkylaminonaphthalenes as solvent acidity sensors [O] . Amy M. Green, Hannah R. Naughton, Zachariah B. Nealy, -1

机译：羰捻6-酰基-2- dialkylaminonaphthalenes作为溶剂酸度传感器
7. Carbonyl Coordination Chemistry from a New Angle: A Computational Study of a-Carbon Acidity Based on Electrophile Coordination Geometry [O] . -1

机译：从新角度的羰基协调化学方法：基于电子泳机协调几何的碳酸性计算研究

Norfloxacin-derivative functionalized octamolybdate: unusual carbonyl coordination and acidity sensitive luminescence

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