Microwave-assisted, tetrabutylammonium hydroxide catalysed 1,4-addition of water to alpha,beta-unsaturated ketones and alpha,beta-ynones in aqueous solution

Lee Hyejeong; Jun Chul-Ho

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Microwave-assisted, tetrabutylammonium hydroxide catalysed 1,4-addition of water to alpha,beta-unsaturated ketones and alpha,beta-ynones in aqueous solution

机译：微波辅助的氢氧化四丁铵水溶液中的α，β-不饱和酮和α，β-乙炔酮催化水的1,4-加成

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Microwave-assisted, tetrabutylammonium hydroxide catalysed 1,4-addition reactions of water to alpha,beta-unsaturated ketones and alpha,beta-ynones take place efficiently in water. Reactions of the resulting beta-hydroxy ketones lead to the formation of either C-C bondcleavage or annulation products.

机译：微波辅助的四丁基氢氧化铵催化的水在水中有效地发生1,4-加成反应，形成α，β-不饱和酮和α，β-乙酮。生成的β-羟基酮的反应导致C-C键裂解或环化产物的形成。

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《RSC Advances》 |2014年第89期|共5页
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Lee Hyejeong; Jun Chul-Ho;
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正文语种 eng
中图分类化学;
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1. Microwave-assisted, tetrabutylammonium hydroxide catalysed 1,4-addition of water to alpha,beta-unsaturated ketones and alpha,beta-ynones in aqueous solution [J] . Lee Hyejeong, Jun Chul-Ho RSC Advances . 2014,第89期

机译：微波辅助的氢氧化四丁铵水溶液中的α，β-不饱和酮和α，β-乙炔酮催化水的1,4-加成
2. Chromium(III)-Catalyzed Addition of Water and Alcohol to alpha, beta-Unsaturated Ketones for the Synthesis of beta-Hydroxyl and beta-Alkoxyl Ketones in Aqueous Media [J] . Yun Jin-Jin, Liu Xuan-Yu, Deng Wei, The Journal of Organic Chemistry . 2018,第18期

机译：铬（III） - 将水和醇加入α，β-不饱和酮的α-不饱和酮，用于合成含水介质中的β-羟基和β-烷氧基酮
3. Micellar Solution of Sodium Dodecyl Sulfate (SDS) Catalyzes Facile Michael Addition of Amines and Thiols to alpha,beta-Unsaturated Ketones in Water under Neutral Conditions [J] . H.Firouzabadi, N.Iranpoor, A.A.Jafari Advanced synthesis & catalysis . 2005,第5期

机译：十二烷基硫酸钠（SDS）的胶束溶液催化中性条件下水中α，β-不饱和酮的胺和硫醇的迈克尔加成反应
4. 1,4-Addition of Arylboronic Acids to p-Aryl-alpha,beta-unsaturated Ketones and Esters Catalyzed by a Rhodium(I)-chiraphos Complex [C] . Takashi Nishikata, Tetsuji Iyama, Hiroto Tachikawa Symposium on Organometallic Chemistry . 2006

机译：1,4-加入芳基硼酸至p-芳基-α，β-不饱和酮和由铑（I）催化的酯 - 富铬络合物
5. I. Studies on the competitive thermal fragmentation of beta-hydroxyketones: Dehydration vs. formaldehyde elimination. II. Studies on the conjugate addition of Grignard reagents to alpha,beta-unsaturated ketones: Isolation and oxidation of E and Z enols of a ketone. [D] . Logaraj, Sundaram. 1988

机译：I.β-羟基酮竞争性热裂解的研究：脱水与甲醛消除。二。格氏试剂到α，β-不饱和酮上的共轭加成研究：酮的E和Z烯醇的分离和氧化。
6. Studies on the inhibition by alpha-amanitin of single-step addition reactions and productive RNA synthesis catalysed by wheat-germ RNA polymerase II. [O] . L de Mercoyrol, C Job, D Job 1989

机译：研究α-amanitin对小麦胚芽RNA聚合酶II催化的一步加成反应和生产性RNA合成的抑制作用。
7. Stereoretentive Addition of N-tert-Butylsulfonyl-alpha-Amido Silanes to Aldehydes, Ketones, alpha,beta-Unsaturated Esters, and Imines [O] . Mita, Tsuyoshi, Saito, Keisuke, Sugawara, Masumi, 2016

机译：N-叔丁基磺酰基-α-氨基硅烷与醛，酮，α，β-不饱和酯和亚胺的立体定向加成

Microwave-assisted, tetrabutylammonium hydroxide catalysed 1,4-addition of water to alpha,beta-unsaturated ketones and alpha,beta-ynones in aqueous solution

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