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Synthesis of Ni3N/SiO2 nanocomposites and investigation of their intrinsic static and dynamic magnetic properties

机译:Ni3N / SiO2纳米复合材料的合成及其固有静磁和动态磁性能的研究

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摘要

Ni3N/SiO2 nanocomposites were prepared via nitriding of a Ni/SiO2 nanocomposite precursor in flowing ammonia. The intrinsic static and dynamic magnetic properties of the as-prepared samples were investigated with a superconducting quantum interference device and an Agilent N5230A network analyzer, respectively. According to our results, it was found that pure phase nanocrystalline Ni3N could be obtained after the Ni/SiO2 nanocomposite precursor was calcined under a flow of NH3 at 300 degrees C, and the as-obtained nanocrystalline Ni3N is non-ferromagnetic under a static magnetic field and nonmagnetic under a dynamic electromagnetic field.
机译:通过在流动的氨中氮化Ni / SiO2纳米复合材料前驱体制备Ni3N / SiO2纳米复合材料。分别使用超导量子干涉仪和安捷伦N5230A网络分析仪研究了所制备样品的固有静态和动态磁性能。根据我们的结果,发现在Ni / SiO2纳米复合材料前体在300℃的NH3流下煅烧后,可以获得纯相纳米晶Ni3N,并且所获得的纳米晶Ni3N在静态磁场下是非铁磁性的。磁场和动态电磁场下的非磁场。

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