Ligand-free Cu-catalyzed O-arylation of aliphatic diols

Zheng Yufen; Zou Wenxing; Luo Laichun; Chen Jiabei; Lin Songwen; Sun Qi

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Ligand-free Cu-catalyzed O-arylation of aliphatic diols

机译：脂族二醇的无配体铜催化O-芳基化

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摘要

Coupling reaction between aryl iodides and aliphatic diols was realized with a ligand-free copper catalyst under mild conditions. This method was successfully applied in the process of scale-up synthesis of medicinal candidate product EMB-3.

机译：用无配体的铜催化剂在温和的条件下实现了芳基碘化物和脂肪族二醇之间的偶联反应。该方法已成功应用于药物候选产品EMB-3的放大合成过程中。

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《RSC Advances》 |2015年第81期|共5页
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Zheng Yufen; Zou Wenxing; Luo Laichun; Chen Jiabei; Lin Songwen; Sun Qi;
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正文语种 eng
中图分类化学;
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专利

1. Ligand-free Cu-catalyzed O-arylation of aliphatic diols [J] . Zheng Yufen, Zou Wenxing, Luo Laichun, RSC Advances . 2015,第81期

机译：脂族二醇的无配体铜催化O-芳基化
2. Efficient Cu-catalyzed intramolecular O-arylation for synthesis of benzoxazoles in water [J] . Yanling Tang, Minxin Li, Hui Gao, RSC Advances . 2020,第24期

机译：高效Cu催化的分子内O-芳基合成苯并恶唑在水中的合成
3. Cu-Catalyzed N- and O-Arylation of 2-, 3-, and 4-Hydroxypyridines and Hydroxyquinolines [J] . Ryan A. Altman, Stephen L. Buchwald Organic letters . 2007,第4期

机译：铜催化的2-，3-和4-羟基吡啶和羟基喹啉的N-和O-芳基化
4. Addition effect of aliphatic monools and diols on the conductivity enhancement of poly(3,4-ethylenedioxythiophene) doped with poly(styrene sulfonic acid) (PEDOT:PSS) [C] . Shigeji Konagaya, Misako Mutou, Mariko Terada International Conference of the Polymer Processing Society . 2019

机译：脂族金属脂族金属和二醇对聚（苯乙烯磺酸）（PEDOT：PSS）掺杂聚（3,4-亚乙基氧噻吩）的电导率增强的添加效果
5. Part I: The Study of 2-Aryl-1,3-Dithiane Derivatives As Pronucleophiles in Palladium-Catalyzed Allylic Alkylation and Propellylation Part II: Ligand-Free Palladium-Catalyzed Allylic Amintion of Hydrazone Derivatives Part III: Synthesis of Criegee Intermed [D] . Trongsiriwat, Nisalak. 2019

机译：第一部分：将2-芳基-1,3-二硫醚衍生物的研究作为钯催化的烯丙基烷基化和预选型第II部分：腙衍生物的配体钯催化烯丙基胺部分III：Criaegee中间的合成
6. A Recyclable Cu-MOF-74 Catalyst for the Ligand-Free O-Arylation Reaction of 4-Nitrobenzaldehyde and Phenol [O] . Pedro Leo, Gisela Orcajo, David Briones, 2017

机译：一种可回收的Cu-MOF-74催化剂用于4-硝基苯甲醛和苯酚的无配体O-芳基化反应
7. Efficient Cu-catalyzed intramolecular O-arylation for synthesis of benzoxazoles in water [O] . Yanling Tang, Minxin Li, Hui Gao, 2020

机译：高效Cu催化的分子内O-芳基合成苯并恶唑在水中的合成

Ligand-free Cu-catalyzed O-arylation of aliphatic diols

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