Synthesis of oxazolidinofullerenes/thiazolidinofullerenes: novel reaction of [60] fullerene with isocyanates/isothiocyanates promoted by ferric perchlorate

Li Fa-Bao; Zhu Ye-Fei; Zhang Xiao-Feng; Shi Ji-Long; Wu Jun; Chen Liu; Liang Xiao-Xue; Liu Li

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Synthesis of oxazolidinofullerenes/thiazolidinofullerenes: novel reaction of [60] fullerene with isocyanates/isothiocyanates promoted by ferric perchlorate

机译：恶唑烷富勒烯/噻唑烷富勒烯的合成：[60]富勒烯与高氯酸铁促进的异氰酸酯/异硫氰酸酯的新型反应

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The facile one-step reaction of [60] fullerene with isocyanates/isothiocyanates in the presence of ferric perchlorate generates a series of oxazolidinofullerenes/thiazolidinofullerenes, which are difficult to prepare by common methods. The direct dissolution approach plays an important role in the efficient synthesis of oxazolidinofullerenes/thiazolidinofullerenes. A possible reaction mechanism for the product formation is proposed.

机译：在高氯酸铁存在下，[60]富勒烯与异氰酸酯/异硫氰酸酯的简便一步反应产生了一系列恶唑烷富勒烯/噻唑烷富勒烯，很难用常规方法制备。直接溶解方法在有效合成恶唑烷富勒烯/噻唑烷富勒烯中起重要作用。提出了可能的产物形成反应机理。

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《RSC Advances》 |2014年第89期|共10页
作者
Li Fa-Bao; Zhu Ye-Fei; Zhang Xiao-Feng; Shi Ji-Long; Wu Jun; Chen Liu; Liang Xiao-Xue; Liu Li;
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正文语种 eng
中图分类化学;
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1. Synthesis of oxazolidinofullerenes/thiazolidinofullerenes: novel reaction of [60] fullerene with isocyanates/isothiocyanates promoted by ferric perchlorate [J] . Li Fa-Bao, Zhu Ye-Fei, Zhang Xiao-Feng, RSC Advances . 2014,第89期

机译：恶唑烷富勒烯/噻唑烷富勒烯的合成：[60]富勒烯与高氯酸铁促进的异氰酸酯/异硫氰酸酯的新型反应
2. Synthesis of disubstituted [60]fullerene-fused lactones: Ferric perchlorate-promoted reaction of [60]fullerene with malonate esters [J] . Li F.-B., You X., Wang G.-W. Organic letters . 2010,第21期

机译：双取代[60]富勒烯稠合内酯的合成：[60]富勒烯与丙二酸酯的高氯酸铁促进反应
3. Synthesis of fullerooxazoles: Novel reactions of [60]fullerene with nitriles promoted by ferric perchlorate [J] . Li FB, Liu TX, Wang GW The Journal of Organic Chemistry . 2008,第16期

机译：Fullerooxazoles的合成：[60]富勒烯与高氯酸铁促进的腈的新反应
4. Synthesis of New Fullerene Dimers and Open-Cage Fullerenes by Solid-State and Liquid-Phase Reactions of C_(60) with N-Containing Aromatics and with Organosilicon Compounds [C] . Koichi Komatsu, Michihisa Murata, Mitsuharu Suzuki, Meeting of the Electrochemical Society . 2002

机译：通过C_（60）与含N芳烃和有机硅化合物的固态和液相反应合成新的富勒烯二聚体和开放式静脉富勒烯
5. Synthesis of cyclic ketene nitrogen,oxygen-acetals and their reactions with isocyanates and isothiocyanates. Nucleophilic substitutions in ionic liquids. [D] . Liu, Zhuqing. 2003

机译：环状烯酮氮，氧-乙缩醛的合成及其与异氰酸酯和异硫氰酸酯的反应。离子液体中的亲核取代。
6. A retro Baeyer–Villiger reaction: electrochemical reduction of 60fullerene-fused lactones to 60fullerene-fused ketones [O] . Chuang Niu, Dian-Bing Zhou, Yong Yang, 2019

机译：Baeyer-Villiger逆反应：将60富勒烯融合的内酯电化学还原为60富勒烯融合的酮
7. Ferric perchlorate-promoted reaction of 60fullerene with β-keto esters [O] . FaBao Li, SanE Zhu, Xun You, 2012

机译：高氯酸铁促进60富勒烯与β-酮酸酯的反应

Synthesis of oxazolidinofullerenes/thiazolidinofullerenes: novel reaction of [60] fullerene with isocyanates/isothiocyanates promoted by ferric perchlorate

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