Gram-scale synthesis of monodisperse Fe nanoparticles in one pot

Haitao Yang; Daiji Hasegawa; Shinsuke Ozaki

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Gram-scale synthesis of monodisperse Fe nanoparticles in one pot

机译：在一锅中克级合成单分散铁纳米颗粒

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A facile synthesis method for monodisperse Fe nanoparticles has been developed by the injection of iron carbonyl into kerosene in one pot. By controlling reaction parameters, 3-12 nm Fe nanoparticles were prepared. The size distribution is very narrow and any size-selective treatment is not required, even when several grams of Fe nanoparticles are synthesized. Magnetic measurements reveal that the saturation magnetization (M_s) of the 9.3 nm Fe nanoparticles is always over 150 emu g~(-1) at room temperature.

机译：通过将羰基铁一锅注入煤油中，已经开发出一种简便的单分散铁纳米颗粒的合成方法。通过控制反应参数，制备了3-12nm的Fe纳米颗粒。尺寸分布非常窄，即使合成了几克的铁纳米颗粒，也不需要任何尺寸选择处理。磁性测量表明，9.3 nm Fe纳米粒子的饱和磁化强度（M_s）在室温下始终超过150 emu g〜（-1）。

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《Scripta materialia》 |2008年第10期|共4页
作者
Haitao Yang; Daiji Hasegawa; Shinsuke Ozaki;
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原文格式 PDF
正文语种 eng
中图分类金属学与热处理;
关键词
Iron nanoparticles; Decomposition; Magnetic properties;

机译：铁纳米粒子分解磁性;

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1. Gram-scale synthesis of monodisperse Fe nanoparticles in one pot [J] . Haitao Yang, Daiji Hasegawa, Shinsuke Ozaki Scripta materialia . 2008,第10期

机译：在一锅中克级合成单分散铁纳米颗粒
2. Gram-Scale Synthesis of Soluble, Near-Monodisperse Gold Nanorods and Other Anisotropic Nanoparticles [J] . Nikhil R. Jana Small . 2005,第8a9期

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3. One-Pot Gram-Scale Synthesis of Hydrogen-Terminated Silicon Nanoparticles [J] . Pujari Sidharam P., Driss Hafedh, Bannani Fatma, Chemistry of Materials: A Publication of the American Chemistry Society . 2018,第18期

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7. One-pot synthesis of monodisperse CoFe2O4@Ag core-shell nanoparticles and their characterization [O] . Shuta Hara, Jumpei Aisu, Masahiro Kato, 2018

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8. Preparation of Monodispersed Fe-Mo Nanoparticles as the Catalyst for CVD Synthesis of Carbon Nanotubes [R] . Li, Y. , Liu, J. , Wang, Y. , 2001

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Gram-scale synthesis of monodisperse Fe nanoparticles in one pot

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