• 主题
高级搜索  >
历史搜索 清空历史
首页> 外文期刊>Separation and Purification Technology >Size-controlled hydrothermal synthesis of SnS2 nanoparticles with high performance in visible light-driven photocatalytic degradation of aqueous methyl orange
【24h】

Size-controlled hydrothermal synthesis of SnS2 nanoparticles with high performance in visible light-driven photocatalytic degradation of aqueous methyl orange

机译：尺寸控制的水热合成SnS2纳米粒子在可见光驱动的甲基橙水溶液的光催化降解中具有高性能

获取原文
获取原文并翻译 | 示例
           
页面导航
  • 摘要
  • 著录项
  • 相似文献
  • 相关主题

摘要

A simple hydrothermal method was developed for the size-controlled synthesis of SnS2 nanoparticles, using common and inexpensive SnCl4-5H2O and thioacetamide as the reactants and 5 vol.% acetic acid aqueous solution as the solvent. The structure, composition and optical property of the obtained products were characterized by X-ray diffraction, transmission electron microscopy, energy dispersive X-ray spectroscopy, X-ray photoelectron spectroscopy, Brumauer-Emmett-Teller (BET) surface area analysis and UV-vis diffuse reflectance spectra, and their possible formation mechanism was proposed. Besides, their photocatalytic properties were tested by degrading methyl orange in distilled water (20 mg/l) under visible light (λ > 420 nm) irradiation. It was found that SnS2 nanoparticles synthesized under the appropriate hydrothermal conditions not only exhibited high visible light-driven photocatalytic activity, but also had good photocatalytic stability.
机译：开发了一种简单的水热方法，用于以尺寸控制的方式合成SnS2纳米粒子，使用常见且价格便宜的SnCl4-5H2O和硫代乙酰胺作为反应物，并使用5体积％的乙酸水溶液作为溶剂。通过X射线衍射，透射电子显微镜，能量色散X射线光谱，X射线光电子能谱，Brumauer-Emmett-Teller（BET）表面积分析和UV-UV表征了所得产物的结构，组成和光学性质。漫反射光谱，并提出了可能的形成机理。此外，通过在可见光（λ> 420 nm）照射下在蒸馏水（20 mg / l）中降解甲基橙来测试其光催化性能。发现在适当的水热条件下合成的SnS2纳米粒子不仅表现出高可见光驱动的光催化活性，而且具有良好的光催化稳定性。

著录项

相似文献

  • 外文文献
  • 中文文献
  • 专利
获取原文

客服邮箱：kefu@zhangqiaokeyan.com

京公网安备：11010802029741号 ICP备案号：京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有

  • 客服微信

  • 服务号