PYRIDINIUM DICHROMATE - A NOVEL REAGENT FOR THE OXIDATION OF STEROIDAL DELTA(5)-3-BETA-ALCOHOLS TO THE CORRESPONDING DELTA(4)-3,6-DIKETONES

Hector M.; Njar VCO.; Hartmann RW.

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PYRIDINIUM DICHROMATE - A NOVEL REAGENT FOR THE OXIDATION OF STEROIDAL DELTA(5)-3-BETA-ALCOHOLS TO THE CORRESPONDING DELTA(4)-3,6-DIKETONES

机译：二氯吡啶鎓-甾体δ（5）-3-BETA醇氧化为相应DEL（4）-3,6-二酮的新型试剂

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A novel procedure for the direct conversion of steroidal Delta(5)-3 beta-alcohols to the corresponding Delta(4)-3,6-diketones in high yield (66-85%) has been achieved using pyridinium dichromate (PDC) in dimethylformamide (DMF) at room temperature. [References: 15]

机译：使用重铬酸吡啶鎓（PDC）实现了将甾族Delta（5）-3β-醇直接转化为相应的Delta（4）-3,6-二酮的高产率（66-85％）的新方法。室温下使用二甲基甲酰胺（DMF）。 [参考：15]

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《Synthetic Communications》 |1996年第6期|共8页
作者
Hector M.; Njar VCO.; Hartmann RW.;
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正文语种 eng
中图分类有机化学;
关键词
Human placental aromatase; Alcohols; Inactivation;

机译：人胎盘芳香酶;酒精;失活;

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1. PYRIDINIUM DICHROMATE - A NOVEL REAGENT FOR THE OXIDATION OF STEROIDAL DELTA(5)-3-BETA-ALCOHOLS TO THE CORRESPONDING DELTA(4)-3,6-DIKETONES [J] . Hector M., Njar VCO., Hartmann RW. Synthetic Communications . 1996,第6期

机译：二氯吡啶鎓-甾体δ（5）-3-BETA醇氧化为相应DEL（4）-3,6-二酮的新型试剂
2. Poly [N-(4-pyridinium dichromate)-P-styrene sulphonamide] as an efficient reagent for oxidation of alcohols [J] . Khazaei A, Mehdipour E, Yadegari S Phosphorus, Sulfur, and Silicon and the Related Elements . 2004,第3期

机译：聚[N-（4-重铬酸吡啶鎓）-P-苯乙烯磺酰胺]作为醇氧化的有效试剂
3. Oxidation of Delta(4)- and Delta(5)-steroids with hydrogen peroxide catalyzed by porphyrin complexes of Mn-III and Fe-III [J] . Rebelo SLH, Simoes MMQ, Neves MGPMS, European journal of organic chemistry . 2004,第23期

机译：Mn-III和Fe-III卟啉配合物催化过氧化氢氧化Delta（4）-和Delta（5）-类固醇
4. Analysis of mice deficient in the bile acid biosynthetic enzyme 3(3-hydroxy-DELTA~5-C_(27)-steroid oxidoreductase (HSD3B7) [C] . H. C. SHEA, K. D. R. SETCHELL, D. W. RUSSEL International Bile Acid Meeting . 2007

机译：胆汁酸生物合成酶3缺乏的小鼠分析（3-羟基 - δ〜5-C_（27） - 蹄氧化还原酶（HSD3B7）
5. Records of delta-carbon-13, delta-oxygen-18 and concentration of atmospheric carbon monoxide in the past. [D] . Wang, Zhihui. 2009

机译：过去记录的δ-碳13，δ-氧18和大气中一氧化碳的浓度。
6. Cumulus cell pappalysin-1 luteinizing hormone/choriogonadotropin receptor amphiregulin and hydroxy-delta-5-steroid dehydrogenase 3 beta- and steroid delta-isomerase 1 mRNA levels associate with oocyte developmental competence and embryo outcomes [O] . Richard J. Kordus, Akhtar Hossain, Michael C. Corso, 2019

机译：积分细胞pappalysin-1叶氏素激素/胆管同时滴黄素受体Amphegegulin和羟化 - Δ-5-类固醇脱氢酶3β-和类固醇δ-异构酶1 mRNA水平与卵母细胞发育能力和胚胎结果相关联
7. Method For Synthesizing 5Beta, 6Beta-Epoxides Of Steroids By A Highly Beta-Selective Epoxidation Of Deltadelta5-Unsaturated Steroids Catalyzed By Ketones [O] . 2005

机译：通过酮催化的Δδ-不饱和甾体的高度β-选择性环氧化合成类固醇的5Beta，6Beta-环氧化物的方法

PYRIDINIUM DICHROMATE - A NOVEL REAGENT FOR THE OXIDATION OF STEROIDAL DELTA(5)-3-BETA-ALCOHOLS TO THE CORRESPONDING DELTA(4)-3,6-DIKETONES

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